thiophosphoric acid O-methyl ester O'-(4-nitro-phenyl) ester O''-(2,3,4,5,6-pentakis-methoxymethoxy-cyclohexyl) ester

Base Information

• Chemical Name: thiophosphoric acid O-methyl ester O'-(4-nitro-phenyl) ester O''-(2,3,4,5,6-pentakis-methoxymethoxy-cyclohexyl) ester
• CAS No.: 206349-77-1
• Molecular Formula: C₂₃H₃₈NO₁₅PS
• Molecular Weight: 631.592

Synonyms:thiophosphoric acid O-methyl ester O'-(4-nitro-phenyl) ester O''-(2,3,4,5,6-pentakis-methoxymethoxy-cyclohexyl) ester

Chemical Property of thiophosphoric acid O-methyl ester O'-(4-nitro-phenyl) ester O''-(2,3,4,5,6-pentakis-methoxymethoxy-cyclohexyl) ester

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Technology Process of thiophosphoric acid O-methyl ester O'-(4-nitro-phenyl) ester O''-(2,3,4,5,6-pentakis-methoxymethoxy-cyclohexyl) ester

There total 3 articles about thiophosphoric acid O-methyl ester O'-(4-nitro-phenyl) ester O''-(2,3,4,5,6-pentakis-methoxymethoxy-cyclohexyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) → thiophosphoric acid O-methyl ester O'-(4-nitro-phenyl) ester O''-(2,3,4,5,6-pentakis-methoxymethoxy-cyclohexyl) ester (206349-77-1)

Guidance literature:

Multi-step reaction with 2 steps

1: CHCl₃ / 0 - 20 °C

2: sulfur / CS₂ / 12 h / 20 °C

With sulfur; In carbon disulfide; chloroform;

DOI:10.1021/ja029362s

Reference yield:

1D-1-O-2,3,4,5,6-(pentakis)methoxymethylene-myo-inositol (153996-50-0) → thiophosphoric acid O-methyl ester O'-(4-nitro-phenyl) ester O''-(2,3,4,5,6-pentakis-methoxymethoxy-cyclohexyl) ester (206349-77-1)

Guidance literature:

Multi-step reaction with 3 steps

1: diisopropylethylamine / CHCl₃ / 6 h / -78 - 20 °C

2: CHCl₃ / 0 - 20 °C

3: sulfur / CS₂ / 12 h / 20 °C

With sulfur; N-ethyl-N,N-diisopropylamine; In carbon disulfide; chloroform;

DOI:10.1021/ja029362s

Reference yield:

Phosphorochloridous acid methyl ester (1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-methoxymethoxy-cyclohexyl ester → thiophosphoric acid O-methyl ester O'-(4-nitro-phenyl) ester O''-(2,3,4,5,6-pentakis-methoxymethoxy-cyclohexyl) ester (206349-77-1)

Guidance literature:

Multi-step reaction with 2 steps

1: CHCl₃ / 0 - 20 °C

2: sulfur / CS₂ / 12 h / 20 °C

With sulfur; In carbon disulfide; chloroform;

DOI:10.1021/ja029362s

upstream raw materials:

4-nitro-phenol

1D-1-O-2,3,4,5,6-(pentakis)methoxymethylene-myo-inositol

Downstream raw materials:

(R)_P-p-nitrophenyl 1-inositol phosphate

(S)-Thiophosphoric acid O-(4-nitro-phenyl) ester O'-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentahydroxy-cyclohexyl) ester

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