2,3-O-(1-methylethylidene)-5,5-di-C-phenyl-α-L-lyxofuranose

Base Information

Chemical Name:2,3-O-(1-methylethylidene)-5,5-di-C-phenyl-α-L-lyxofuranose
CAS No.:581798-56-3
Molecular Formula:C₂₀H₂₂O₅
Molecular Weight:342.392
Hs Code.:

Synonyms:2,3-O-(1-methylethylidene)-5,5-di-C-phenyl-α-L-lyxofuranose

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Chemical Property of 2,3-O-(1-methylethylidene)-5,5-di-C-phenyl-α-L-lyxofuranose

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Technology Process of 2,3-O-(1-methylethylidene)-5,5-di-C-phenyl-α-L-lyxofuranose

There total 6 articles about 2,3-O-(1-methylethylidene)-5,5-di-C-phenyl-α-L-lyxofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 581798-51-8
benzyl 2,3-O-(1-methylethylidene)-5,5-di-C-phenyl-α-L-lyxofuranoside

: 581798-56-3
2,3-O-(1-methylethylidene)-5,5-di-C-phenyl-α-L-lyxofuranose

Guidance literature:: With hydrogen; palladium on activated charcoal; In diethyl ether; for 12h; under 3075.25 Torr;
DOI:10.1021/ol034796t

Reference yield:

: 100-59-4
phenylmagnesium chloride

: 581798-56-3
2,3-O-(1-methylethylidene)-5,5-di-C-phenyl-α-L-lyxofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / diethyl ether / 2 h / Heating

2: hydrogen / Pd/C / diethyl ether / 12 h / 3075.25 Torr

With hydrogen; palladium on activated charcoal; In diethyl ether;
DOI:10.1021/ol034796t

Reference yield:

: 74912-02-0
phenylmethyl-2,3-O-(1-methylethylidene)-β-D-gulofuranoside

: 581798-56-3
2,3-O-(1-methylethylidene)-5,5-di-C-phenyl-α-L-lyxofuranose

Guidance literature:: Multi-step reaction with 5 steps

1: sodium periodate / methanol; H₂O / 2 h / 20 °C

2: silver nitrate; potassium hydroxide / H₂O; ethanol / 6 h

3: diethyl ether / 0 °C

4: 82 percent / diethyl ether / 2 h / Heating

5: hydrogen / Pd/C / diethyl ether / 12 h / 3075.25 Torr

With potassium hydroxide; sodium periodate; hydrogen; silver nitrate; palladium on activated charcoal; In methanol; diethyl ether; ethanol; water;
DOI:10.1021/ol034796t