p-dimethylsilylbenzaldehyde

Base Information

Chemical Name:p-dimethylsilylbenzaldehyde
CAS No.:129731-03-9
Molecular Formula:C₉H₁₂OSi
Molecular Weight:164.279
Hs Code.:

Synonyms:p-dimethylsilylbenzaldehyde

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Chemical Property of p-dimethylsilylbenzaldehyde

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Technology Process of p-dimethylsilylbenzaldehyde

There total 3 articles about p-dimethylsilylbenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1637-65-6
4-dimethylsilylphenylmagnesium bromide

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 129731-03-9
p-dimethylsilylbenzaldehyde

Guidance literature:: 4-dimethylsilylphenylmagnesium bromide; With magnesium; In tetrahydrofuran; ethylene dibromide; at 20 ℃; for 2h; Inert atmosphere;

N,N-dimethyl-formamide; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 2h; Inert atmosphere;

Reference yield: 7.0%

: 116088-83-6
(p-Cyanophenyl)dimethylchlorosilane

: 129731-03-9
p-dimethylsilylbenzaldehyde

: 129409-68-3
4-(dimethylsilyl)benzonitrile

Guidance literature:: With diisobutylaluminium hydride; In tetrahydrofuran; at 0 ℃; for 0.333333h;

Reference yield:

: 106-37-6
1.4-dibromobenzene

: 129731-03-9
p-dimethylsilylbenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium; isopropylmagnesium chloride / 2 h / -5 °C / Inert atmosphere

1.2: 2 h / 20 °C / Inert atmosphere

2.1: magnesium / tetrahydrofuran; ethylene dibromide / 2 h / 20 °C / Inert atmosphere

2.2: 2 h / 0 - 20 °C / Inert atmosphere

With n-butyllithium; isopropylmagnesium chloride; magnesium; In tetrahydrofuran; ethylene dibromide;