benzyloxycarbonylmethyl 2-deoxy-2-tetradecanoylamino-α-D-glucopyranoside

Base Information

Chemical Name:benzyloxycarbonylmethyl 2-deoxy-2-tetradecanoylamino-α-D-glucopyranoside
CAS No.:120720-68-5
Molecular Formula:C₂₉H₄₇NO₈
Molecular Weight:537.694
Hs Code.:

Synonyms:benzyloxycarbonylmethyl 2-deoxy-2-tetradecanoylamino-α-D-glucopyranoside

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Chemical Property of benzyloxycarbonylmethyl 2-deoxy-2-tetradecanoylamino-α-D-glucopyranoside

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Technology Process of benzyloxycarbonylmethyl 2-deoxy-2-tetradecanoylamino-α-D-glucopyranoside

There total 4 articles about benzyloxycarbonylmethyl 2-deoxy-2-tetradecanoylamino-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 100-39-0
benzyl bromide

: 118638-89-4
carboxymethyl 2-deoxy-2-tetradecanoylamino-α-D-glucopyranoside

: 120720-68-5
benzyloxycarbonylmethyl 2-deoxy-2-tetradecanoylamino-α-D-glucopyranoside

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 60 ℃; for 2h;
DOI:10.1248/cpb.39.3244

Reference yield:

: ((2S,3R,4R,5S,6R)-4,5-Diacetoxy-6-acetoxymethyl-3-amino-tetrahydro-pyran-2-yloxy)-acetic acid methyl ester

: 120720-68-5
benzyloxycarbonylmethyl 2-deoxy-2-tetradecanoylamino-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: N-methylmorpholine / CH₂Cl₂ / 1 h

2: 93 percent / 1 M aq. NaOH / tetrahydrofuran / 0.33 h

3: 88 percent / Et₃N / dimethylformamide / 2 h / 60 °C

With 4-methyl-morpholine; sodium hydroxide; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1248/cpb.39.3244

Reference yield:

: 118662-72-9
methoxycarbonylmethyl 3,4,6-tri-O-acetyl-2-deoxy-2-tetradecanoylamino-α-D-glucopyranoside

: 120720-68-5
benzyloxycarbonylmethyl 2-deoxy-2-tetradecanoylamino-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / 1 M aq. NaOH / tetrahydrofuran / 0.33 h

2: 88 percent / Et₃N / dimethylformamide / 2 h / 60 °C

With sodium hydroxide; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1248/cpb.39.3244