benzyloxycarbonylmethyl 2-deoxy-4,6-O-isopropylidene-2-tetradecanoylamino-α-D-glucopyranoside

Base Information

Chemical Name:benzyloxycarbonylmethyl 2-deoxy-4,6-O-isopropylidene-2-tetradecanoylamino-α-D-glucopyranoside
CAS No.:118638-90-7
Molecular Formula:C₃₂H₅₁NO₈
Molecular Weight:577.759
Hs Code.:

Synonyms:benzyloxycarbonylmethyl 2-deoxy-4,6-O-isopropylidene-2-tetradecanoylamino-α-D-glucopyranoside

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Chemical Property of benzyloxycarbonylmethyl 2-deoxy-4,6-O-isopropylidene-2-tetradecanoylamino-α-D-glucopyranoside

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Technology Process of benzyloxycarbonylmethyl 2-deoxy-4,6-O-isopropylidene-2-tetradecanoylamino-α-D-glucopyranoside

There total 6 articles about benzyloxycarbonylmethyl 2-deoxy-4,6-O-isopropylidene-2-tetradecanoylamino-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 120720-68-5
benzyloxycarbonylmethyl 2-deoxy-2-tetradecanoylamino-α-D-glucopyranoside

: 77-76-9
2,2-dimethoxy-propane

: 118638-90-7
benzyloxycarbonylmethyl 2-deoxy-4,6-O-isopropylidene-2-tetradecanoylamino-α-D-glucopyranoside

Guidance literature:: With toluene-4-sulfonic acid; In N,N-dimethyl-formamide; for 3.5h;
DOI:10.1248/cpb.39.3244

Reference yield:

: 100-39-0
benzyl bromide

: 118638-90-7
benzyloxycarbonylmethyl 2-deoxy-4,6-O-isopropylidene-2-tetradecanoylamino-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / Et₃N / dimethylformamide / 2 h / 60 °C

2: 89 percent / p-TsOH*H₂O / dimethylformamide / 3.5 h

With toluene-4-sulfonic acid; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1248/cpb.39.3244

Reference yield:

: ((2S,3R,4R,5S,6R)-4,5-Diacetoxy-6-acetoxymethyl-3-amino-tetrahydro-pyran-2-yloxy)-acetic acid methyl ester

: 118638-90-7
benzyloxycarbonylmethyl 2-deoxy-4,6-O-isopropylidene-2-tetradecanoylamino-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: N-methylmorpholine / CH₂Cl₂ / 1 h

2: 93 percent / 1 M aq. NaOH / tetrahydrofuran / 0.33 h

3: 88 percent / Et₃N / dimethylformamide / 2 h / 60 °C

4: 89 percent / p-TsOH*H₂O / dimethylformamide / 3.5 h

With 4-methyl-morpholine; sodium hydroxide; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1248/cpb.39.3244