4-chlorophenyl 4-cyanophenyl selenide

Base Information

• Chemical Name: 4-chlorophenyl 4-cyanophenyl selenide
• CAS No.: 1253853-25-6
• Molecular Formula: C₁₃H₈ClNSe
• Molecular Weight: 292.626
• Mol file: 1253853-25-6.mol

Synonyms:4-chlorophenyl 4-cyanophenyl selenide

Chemical Property of 4-chlorophenyl 4-cyanophenyl selenide

Chemical Property:

Purity/Quality:

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Technology Process of 4-chlorophenyl 4-cyanophenyl selenide

There total 2 articles about 4-chlorophenyl 4-cyanophenyl selenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

4-bromobenzenecarbonitrile (623-00-7) + 4-chlorophenylselenotributylstannane (1253853-23-4) → 4-chlorophenyl 4-cyanophenyl selenide (1253853-25-6)

Guidance literature:

With [Cu2(μ-I)2(1,10-phenanthroline)2]; In N,N-dimethyl-formamide; at 140 ℃; for 0.2h; Microwave irradiation;

DOI:10.1246/cl.2010.720

Reference yield: 90.0%

bis(p-chlorophenyl) diselenide (20541-49-5) + 4-cyanophenylboronic acid (126747-14-6) → 4-chlorophenyl 4-cyanophenyl selenide (1253853-25-6)

Guidance literature:

With MCM-41 immobilized bipyridine copper(I) complex; In water; dimethyl sulfoxide; at 110 ℃; for 14h; Schlenk technique; Green chemistry;

DOI:10.1039/c4nj01687d

upstream raw materials:

4-bromobenzenecarbonitrile

4-chlorophenylselenotributylstannane

bis(p-chlorophenyl) diselenide

4-cyanophenylboronic acid