2,3-dimethylbutan-2-amine hydrochloride (1:1)

Base Information

Chemical Name:2,3-dimethylbutan-2-amine hydrochloride (1:1)
CAS No.:29772-69-8
Molecular Formula:C6H15 N . Cl H
Molecular Weight:137.653
Hs Code.:
Mol file:29772-69-8.mol

Synonyms:2-Butanamine,2,3-dimethyl-, hydrochloride (9CI); Propylamine, 1,1,2-trimethyl-,hydrochloride (7CI,8CI)

Suppliers and Price of 2,3-dimethylbutan-2-amine hydrochloride (1:1)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 2,3-dimethylbutan-2-amine hydrochloride (1:1)

Chemical Property:

Vapor Pressure:30.8mmHg at 25°C
Boiling Point:104.5°C at 760 mmHg
Flash Point:7.5°C

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,3-dimethylbutan-2-amine hydrochloride (1:1)

There total 4 articles about 2,3-dimethylbutan-2-amine hydrochloride (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 79-29-8
2,3-dimethylbutane

: 29772-69-8
1,1,2-trimethylpropylamine hydrochloride

Guidance literature:: 2,3-dimethylbutane; With Benzophenone imine; iodobenzene dimethoxide; at 75 ℃; for 24h; Inert atmosphere;

With hydrogenchloride; In methanol; water; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1002/chem.202102627

Reference yield: 27.0%

: 78-82-0
Isobutyronitrile

: 676-58-4
methylmagnesium chloride

: 29772-69-8
1,1,2-trimethylpropylamine hydrochloride

Guidance literature:: Isobutyronitrile; methylmagnesium chloride; titanium(IV) isopropylate; In diethyl ether; at 20 ℃;

With hydrogenchloride; In diethyl ether; dichloromethane; Further stages.;
DOI:10.1134/S1070428007100016

Reference yield:

: 79-29-8
2,3-dimethylbutane

: 29772-69-8
1,1,2-trimethylpropylamine hydrochloride

: 89585-12-6
2,3-dimethylbutan-1-amine hydrochloride

Guidance literature:: 2,3-dimethylbutane; With cerium(III) chloride; 1,1,1-trichloroethanol; di-tert-butyl-diazodicarboxylate; tetrabutyl-ammonium chloride; In acetonitrile; at 20 ℃; for 18h; Irradiation; Inert atmosphere; Sealed tube;

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h; Reagent/catalyst; Further stages;
DOI:10.1021/jacs.0c00212