8-amino-6-methoxy-4-methyl-5-phenyloxyquinoline

Base Information

Chemical Name:8-amino-6-methoxy-4-methyl-5-phenyloxyquinoline
CAS No.:82329-71-3
Molecular Formula:C₁₇H₁₆N₂O₂
Molecular Weight:280.326
Hs Code.:

Synonyms:8-amino-6-methoxy-4-methyl-5-phenyloxyquinoline

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Chemical Property of 8-amino-6-methoxy-4-methyl-5-phenyloxyquinoline

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Technology Process of 8-amino-6-methoxy-4-methyl-5-phenyloxyquinoline

There total 5 articles about 8-amino-6-methoxy-4-methyl-5-phenyloxyquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 82329-60-0
6-methoxy-4-methyl-8-nitro-5-phenyloxyquinoline

: 82329-71-3
8-amino-6-methoxy-4-methyl-5-phenyloxyquinoline

Guidance literature:: With iron; acetic acid; In water; for 2h; Reflux;
DOI:10.1016/j.bmcl.2014.05.085

Reference yield:

: 7357-66-6
N-(5-bromo-4-methoxy-2-nitrophenyl)acetamide

: 82329-71-3
8-amino-6-methoxy-4-methyl-5-phenyloxyquinoline

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium tert-butylate / tert-butyl alcohol / 12 h / 25 °C / Inert atmosphere

1.2: 24 h / 60 - 120 °C / Inert atmosphere

2.1: hydrogenchloride / ethanol / 2 h / Reflux

3.1: orthoarsenic acid; phosphoric acid / 0.5 h / 120 °C

4.1: acetic acid; iron / water / 2 h / Reflux

With hydrogenchloride; phosphoric acid; potassium tert-butylate; orthoarsenic acid; iron; acetic acid; In ethanol; water; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2014.05.085

Reference yield:

: 108-95-2,27073-41-2
phenol

: 82329-71-3
8-amino-6-methoxy-4-methyl-5-phenyloxyquinoline

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium tert-butylate / tert-butyl alcohol / 12 h / 25 °C / Inert atmosphere

1.2: 24 h / 60 - 120 °C / Inert atmosphere

2.1: hydrogenchloride / ethanol / 2 h / Reflux

3.1: orthoarsenic acid; phosphoric acid / 0.5 h / 120 °C

4.1: acetic acid; iron / water / 2 h / Reflux

With hydrogenchloride; phosphoric acid; potassium tert-butylate; orthoarsenic acid; iron; acetic acid; In ethanol; water; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2014.05.085