N-(1,1,3,3-Tetramethylbutyl)-N-(2,2,4,4-tetramethyltetramethylene)sulfamide

Base Information

• Chemical Name: N-(1,1,3,3-Tetramethylbutyl)-N-(2,2,4,4-tetramethyltetramethylene)sulfamide
• CAS No.: 76613-37-1
• Molecular Formula: C₁₆H₃₄N₂O₂S
• Molecular Weight: 318.524
• Mol file: 76613-37-1.mol

Synonyms:N-(1,1,3,3-Tetramethylbutyl)-N-(2,2,4,4-tetramethyltetramethylene)sulfamide

Chemical Property of N-(1,1,3,3-Tetramethylbutyl)-N-(2,2,4,4-tetramethyltetramethylene)sulfamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(1,1,3,3-Tetramethylbutyl)-N-(2,2,4,4-tetramethyltetramethylene)sulfamide

There total 2 articles about N-(1,1,3,3-Tetramethylbutyl)-N-(2,2,4,4-tetramethyltetramethylene)sulfamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

N,N'-bis(1,1,3,3-tetramethylbutyl)thiadiaziridine 1,1-dioxide (50780-12-6,40121-15-1) + phenyl isocyanate (103-71-9) → 2,2,4,4-Tetramethyl-1-phenylcarbamoyl-pyrrolidin (76613-38-2) + N-(1,1,3,3-Tetramethylbutyl)-N-(2,2,4,4-tetramethyltetramethylene)sulfamide (76613-37-1)

Guidance literature:

for 72h; Heating;

DOI:10.1021/jo00323a021

Reference yield:

N,N'-bis(1,1,3,3-tetramethylbutyl)thiadiaziridine 1,1-dioxide (50780-12-6,40121-15-1) → N,N'-bis(1,1,3,3-tetramethylbutyl)sulfamide (6281-65-8) + N-(1,1,3,3-Tetramethylbutyl)-N-(2,2,4,4-tetramethyltetramethylene)sulfamide (76613-37-1)

Guidance literature:

With thiophenol; In benzene; for 4h; Heating;

DOI:10.1021/jo00323a021

Reference yield: 68.0%

N-(1,1,3,3-Tetramethylbutyl)-N-(2,2,4,4-tetramethyltetramethylene)sulfamide (76613-37-1) + phenyl isocyanate (103-71-9) → 2,2,4,4-Tetramethyl-1-phenylcarbamoyl-pyrrolidin (76613-38-2) + N-carboethoxyaniline (101-99-5)

Guidance literature:

In benzene; 1) reflux, 72 h, 2) EtOH, reflux, 1 h;

DOI:10.1021/jo00153a033

upstream raw materials:

N,N'-bis(1,1,3,3-tetramethylbutyl)thiadiaziridine 1,1-dioxide

phenyl isocyanate

Downstream raw materials:

2,2,4,4-Tetramethyl-1-phenylcarbamoyl-pyrrolidin

N-carboethoxyaniline