Trithiocarbonic acid 2-([1,3]dithiolan-2-ylsulfanyl)-ethyl ester ethyl ester

Base Information

Chemical Name:Trithiocarbonic acid 2-([1,3]dithiolan-2-ylsulfanyl)-ethyl ester ethyl ester
CAS No.:78186-87-5
Molecular Formula:C₈H₁₄S₆
Molecular Weight:302.595
Hs Code.:

Synonyms:Trithiocarbonic acid 2-([1,3]dithiolan-2-ylsulfanyl)-ethyl ester ethyl ester

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Chemical Property of Trithiocarbonic acid 2-([1,3]dithiolan-2-ylsulfanyl)-ethyl ester ethyl ester

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Technology Process of Trithiocarbonic acid 2-([1,3]dithiolan-2-ylsulfanyl)-ethyl ester ethyl ester

There total 1 articles about Trithiocarbonic acid 2-([1,3]dithiolan-2-ylsulfanyl)-ethyl ester ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 33145-02-7
2,2'-<1,2-ethanediylbis(thio)>bis-1,3-dithiolane

: 75-03-6
ethyl iodide

: 822-38-8
1,3-dithiolane-2-thione

: 57443-64-8
1,2-ethanediyl bis(ethyl trithiocarbonate)

: 78186-87-5
Trithiocarbonic acid 2-([1,3]dithiolan-2-ylsulfanyl)-ethyl ester ethyl ester

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, -5-(-10) grad C, 30 min, nitrogen, 2.) THF, 1 h at -5-(-10) grad C then 24 h at room temp.;
DOI:10.1016/S0040-4039(01)92515-8