beta,4-Dimethoxy-3-(phenylmethoxy)benzeneethanamine

Base Information

Chemical Name:beta,4-Dimethoxy-3-(phenylmethoxy)benzeneethanamine
CAS No.:29973-93-1
Molecular Formula:C₁₇H₂₁NO₃
Molecular Weight:287.359
Hs Code.:
DSSTox Substance ID:DTXSID201240455

Synonyms:29973-93-1;beta,4-Dimethoxy-3-(phenylmethoxy)benzeneethanamine;DTXSID201240455

Suppliers and Price of beta,4-Dimethoxy-3-(phenylmethoxy)benzeneethanamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of beta,4-Dimethoxy-3-(phenylmethoxy)benzeneethanamine

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:7
Exact Mass:287.15214353
Heavy Atom Count:21
Complexity:281

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)C(CN)OC)OCC2=CC=CC=C2

Technology Process of beta,4-Dimethoxy-3-(phenylmethoxy)benzeneethanamine

There total 5 articles about beta,4-Dimethoxy-3-(phenylmethoxy)benzeneethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 29973-92-0
2-(benzyloxy)-1-methoxy-4-(1-methoxy-2-nitroethyl) Benzene

: 29973-93-1
2-(3-(benzyloxy)-4-methoxyphenyl)-2-methoxyethan-1-amine

Guidance literature:: With hydrogenchloride; zinc; In tetrahydrofuran; methanol; for 10h; Reflux;

Reference yield:

: 63909-29-5,55507-05-6
3-benzyloxy-4-methoxy-β-nitrostyrene

: 29973-93-1
2-(3-(benzyloxy)-4-methoxyphenyl)-2-methoxyethan-1-amine

Guidance literature:: Multi-step reaction with 2 steps

1: methanol. sodium methylate

2: LiAlH₄; diethyl ether

With lithium aluminium tetrahydride; diethyl ether; sodium methylate;
DOI:10.1002/ardp.19562890705

Reference yield:

: 6346-05-0
3-benzyloxy-4-methoxybenzaldehyde

: 29973-93-1
2-(3-(benzyloxy)-4-methoxyphenyl)-2-methoxyethan-1-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / NH₄OAc / acetic acid / 2 h / Heating

2: 62 percent / Na / CH₂Cl₂ / 0.08 h / Ambient temperature

3: 8.45 g / LiAlH₄ / diethyl ether; tetrahydrofuran / 3.5 h / Heating

With lithium aluminium tetrahydride; ammonium acetate; sodium; In tetrahydrofuran; diethyl ether; dichloromethane; acetic acid;
DOI:10.1016/S0040-4020(97)00287-1