2-(4-(benzyloxy)-3-methoxyphenyl)-N-(2-(3-(benzyloxy)-4-methoxyphenyl)-2-methoxyethyl)acetamide

Base Information

Chemical Name:2-(4-(benzyloxy)-3-methoxyphenyl)-N-(2-(3-(benzyloxy)-4-methoxyphenyl)-2-methoxyethyl)acetamide
CAS No.:35320-04-8
Molecular Formula:C₃₃H₃₅NO₆
Molecular Weight:541.644
Hs Code.:

Synonyms:2-(4-(benzyloxy)-3-methoxyphenyl)-N-(2-(3-(benzyloxy)-4-methoxyphenyl)-2-methoxyethyl)acetamide

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Chemical Property of 2-(4-(benzyloxy)-3-methoxyphenyl)-N-(2-(3-(benzyloxy)-4-methoxyphenyl)-2-methoxyethyl)acetamide

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Technology Process of 2-(4-(benzyloxy)-3-methoxyphenyl)-N-(2-(3-(benzyloxy)-4-methoxyphenyl)-2-methoxyethyl)acetamide

There total 5 articles about 2-(4-(benzyloxy)-3-methoxyphenyl)-N-(2-(3-(benzyloxy)-4-methoxyphenyl)-2-methoxyethyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 29973-91-9
4-benzyloxy-3-methoxyphenylacetic acid

: 29973-93-1
2-(3-(benzyloxy)-4-methoxyphenyl)-2-methoxyethan-1-amine

: 35320-04-8
2-(4-(benzyloxy)-3-methoxyphenyl)-N-(2-(3-(benzyloxy)-4-methoxyphenyl)-2-methoxyethyl)acetamide

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 48h; Cooling; Inert atmosphere;
DOI:10.1021/acs.joc.7b01061

Reference yield:

: 29973-92-0
2-(benzyloxy)-1-methoxy-4-(1-methoxy-2-nitroethyl) Benzene

: 35320-04-8
2-(4-(benzyloxy)-3-methoxyphenyl)-N-(2-(3-(benzyloxy)-4-methoxyphenyl)-2-methoxyethyl)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 8.45 g / LiAlH₄ / diethyl ether; tetrahydrofuran / 3.5 h / Heating

2: 1.) DCC / 1.) CH₂Cl₂, 0 deg C, 25 min, 2.) CH₂Cl₂, room temp., overnight

With lithium aluminium tetrahydride; dicyclohexyl-carbodiimide; In tetrahydrofuran; diethyl ether;
DOI:10.1016/S0040-4020(97)00287-1

Reference yield:

: 6346-05-0
3-benzyloxy-4-methoxybenzaldehyde

: 35320-04-8
2-(4-(benzyloxy)-3-methoxyphenyl)-N-(2-(3-(benzyloxy)-4-methoxyphenyl)-2-methoxyethyl)acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: 81 percent / NH₄OAc / acetic acid / 2 h / Heating

2: 62 percent / Na / CH₂Cl₂ / 0.08 h / Ambient temperature

3: 8.45 g / LiAlH₄ / diethyl ether; tetrahydrofuran / 3.5 h / Heating

4: 1.) DCC / 1.) CH₂Cl₂, 0 deg C, 25 min, 2.) CH₂Cl₂, room temp., overnight

With lithium aluminium tetrahydride; ammonium acetate; sodium; dicyclohexyl-carbodiimide; In tetrahydrofuran; diethyl ether; dichloromethane; acetic acid;
DOI:10.1016/S0040-4020(97)00287-1