2-Benzyloxy-1-methoxy-4-(1-methoxy-2-nitroethyl)benzene

Base Information

Chemical Name:2-Benzyloxy-1-methoxy-4-(1-methoxy-2-nitroethyl)benzene
CAS No.:29973-92-0
Molecular Formula:C17H19NO5
Molecular Weight:317.342
Hs Code.:
DSSTox Substance ID:DTXSID70700722
Mol file:29973-92-0.mol

Synonyms:2-BENZYLOXY-1-METHOXY-4-(1-METHOXY-2-NITROETHYL)BENZENE;29973-92-0;1-methoxy-4-(1-methoxy-2-nitroethyl)-2-phenylmethoxybenzene;1-Methoxy-1-(3-benzyloxy-4-methoxyphenyl)-2-nitroethane;DTXSID70700722;VHENNGKCCKIURS-UHFFFAOYSA-N;FT-0662946;J-017715;2-(Benzyloxy)-1-methoxy-4-(1-methoxy-2-nitroethyl)benzene

Suppliers and Price of 2-Benzyloxy-1-methoxy-4-(1-methoxy-2-nitroethyl)benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-Benzyloxy-1-methoxy-4-(1-methoxy-2-nitroethyl)benzene
100 mg
$ 155.00

Biosynth Carbosynth
2-Benzyloxy-1-methoxy-4-(1-methoxy-2-nitroethyl)benzene
250 mg
$ 462.50

Biosynth Carbosynth
2-Benzyloxy-1-methoxy-4-(1-methoxy-2-nitroethyl)benzene
100 mg
$ 255.00

Biosynth Carbosynth
2-Benzyloxy-1-methoxy-4-(1-methoxy-2-nitroethyl)benzene
50 mg
$ 140.00

Biosynth Carbosynth
2-Benzyloxy-1-methoxy-4-(1-methoxy-2-nitroethyl)benzene
1 g
$ 1528.80

Biosynth Carbosynth
2-Benzyloxy-1-methoxy-4-(1-methoxy-2-nitroethyl)benzene
500 mg
$ 840.00

American Custom Chemicals Corporation
2-BENZYLOXY-1-METHOXY-4-(1-METHOXY-2-NITROETHYL)BENZENE 95.00%
5MG
$ 505.43

AK Scientific
2-Benzyloxy-1-methoxy-4-(1-methoxy-2-nitroethyl)benzene
500mg
$ 1184.00

Total 4 raw suppliers

Chemical Property of 2-Benzyloxy-1-methoxy-4-(1-methoxy-2-nitroethyl)benzene

Chemical Property:

Melting Point:99 °C(Solv: ethanol (64-17-5))
Boiling Point:452.6±45.0 °C(Predicted)
PKA:7.78±0.38(Predicted)
PSA：73.51000
Density:1.186±0.06 g/cm3(Predicted)
LogP:3.76160
Solubility.:Chloroform, Dichloromethane, Ethyl Acetate
XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:7
Exact Mass:317.12632271
Heavy Atom Count:23
Complexity:353

Purity/Quality:

98% ^*data from raw suppliers

2-Benzyloxy-1-methoxy-4-(1-methoxy-2-nitroethyl)benzene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)C(C[N+](=O)[O-])OC)OCC2=CC=CC=C2
Uses Papaverine intermediate.

Technology Process of 2-Benzyloxy-1-methoxy-4-(1-methoxy-2-nitroethyl)benzene

There total 6 articles about 2-Benzyloxy-1-methoxy-4-(1-methoxy-2-nitroethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 63909-29-5,55507-05-6
3-benzyloxy-4-methoxy-β-nitrostyrene

: 124-41-4
sodium methylate

: 29973-92-0
2-(benzyloxy)-1-methoxy-4-(1-methoxy-2-nitroethyl) Benzene

Guidance literature:: In methanol; dichloromethane; at 20 ℃; for 0.133333h; Inert atmosphere;
DOI:10.1021/acs.joc.7b01061

Reference yield: 62.0%

: 67-56-1
methanol

: 63909-29-5
(E)-2-(benzyloxy)-1-methoxy-4-(2-nitrovinyl)benzene

: 29973-92-0
2-(benzyloxy)-1-methoxy-4-(1-methoxy-2-nitroethyl) Benzene

Guidance literature:: With sodium; In dichloromethane; for 0.0833333h; Ambient temperature;
DOI:10.1016/S0040-4020(97)00287-1

Reference yield:

: 6346-05-0
3-benzyloxy-4-methoxybenzaldehyde

: 29973-92-0
2-(benzyloxy)-1-methoxy-4-(1-methoxy-2-nitroethyl) Benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / NH₄OAc / acetic acid / 2 h / Heating

2: 62 percent / Na / CH₂Cl₂ / 0.08 h / Ambient temperature

With ammonium acetate; sodium; In dichloromethane; acetic acid;
DOI:10.1016/S0040-4020(97)00287-1