((S)-1-{(S)-1-[(S)-2-tert-Butoxycarbonylamino-1-(methoxy-methyl-carbamoyl)-ethylcarbamoyl]-2-phenyl-ethylcarbamoyl}-3-methyl-butyl)-carbamic acid benzyl ester

Base Information

Chemical Name:((S)-1-{(S)-1-[(S)-2-tert-Butoxycarbonylamino-1-(methoxy-methyl-carbamoyl)-ethylcarbamoyl]-2-phenyl-ethylcarbamoyl}-3-methyl-butyl)-carbamic acid benzyl ester
CAS No.:211756-50-2
Molecular Formula:C₃₃H₄₇N₅O₈
Molecular Weight:641.765
Hs Code.:

((S)-1-{(S)-1-[(S)-2-tert-Butoxycarbonylamino-1-(methoxy-methyl-carbamoyl)-ethylcarbamoyl]-2-phenyl-ethylcarbamoyl}-3-methyl-butyl)-carbamic acid benzyl ester

Synonyms:((S)-1-{(S)-1-[(S)-2-tert-Butoxycarbonylamino-1-(methoxy-methyl-carbamoyl)-ethylcarbamoyl]-2-phenyl-ethylcarbamoyl}-3-methyl-butyl)-carbamic acid benzyl ester

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Chemical Property of ((S)-1-{(S)-1-[(S)-2-tert-Butoxycarbonylamino-1-(methoxy-methyl-carbamoyl)-ethylcarbamoyl]-2-phenyl-ethylcarbamoyl}-3-methyl-butyl)-carbamic acid benzyl ester

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Technology Process of ((S)-1-{(S)-1-[(S)-2-tert-Butoxycarbonylamino-1-(methoxy-methyl-carbamoyl)-ethylcarbamoyl]-2-phenyl-ethylcarbamoyl}-3-methyl-butyl)-carbamic acid benzyl ester

There total 5 articles about ((S)-1-{(S)-1-[(S)-2-tert-Butoxycarbonylamino-1-(methoxy-methyl-carbamoyl)-ethylcarbamoyl]-2-phenyl-ethylcarbamoyl}-3-methyl-butyl)-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 211756-50-2
((S)-1-{(S)-1-[(S)-2-tert-Butoxycarbonylamino-1-(methoxy-methyl-carbamoyl)-ethylcarbamoyl]-2-phenyl-ethylcarbamoyl}-3-methyl-butyl)-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / aq. NaOH / 2-methyl-propan-2-ol / 12 h / Ambient temperature

2: 89 percent / EDCI, 4-methylmorpholine / CH₂Cl₂ / 12 h / Ambient temperature

3: H₂ / 10percent Pd/C / methanol / 2 h

4: dimethylformamide; CH₂Cl₂ / Ambient temperature

With 4-methyl-morpholine; sodium hydroxide; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/jm980071x

Reference yield:

: 16947-84-5,62234-36-0
N-[(benzyloxy)carbonyl]-3-[(tert-butoxycarbonyl)amino]-L-alanine

: 211756-50-2
((S)-1-{(S)-1-[(S)-2-tert-Butoxycarbonylamino-1-(methoxy-methyl-carbamoyl)-ethylcarbamoyl]-2-phenyl-ethylcarbamoyl}-3-methyl-butyl)-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / EDCI, 4-methylmorpholine / CH₂Cl₂ / 12 h / Ambient temperature

2: H₂ / 10percent Pd/C / methanol / 2 h

3: dimethylformamide; CH₂Cl₂ / Ambient temperature

With 4-methyl-morpholine; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm980071x

Reference yield:

: 173259-61-5
(S)-2-benzyloxycarbonylamino-3-tert-butoxycarbonylamino-N-methoxy-N-methylpropanamide

: 211756-50-2
((S)-1-{(S)-1-[(S)-2-tert-Butoxycarbonylamino-1-(methoxy-methyl-carbamoyl)-ethylcarbamoyl]-2-phenyl-ethylcarbamoyl}-3-methyl-butyl)-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10percent Pd/C / methanol / 2 h

2: dimethylformamide; CH₂Cl₂ / Ambient temperature

With hydrogen; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm980071x