tert-butyl 3,5-dibromobenzoate

Base Information

Chemical Name:tert-butyl 3,5-dibromobenzoate
CAS No.:422569-46-8
Molecular Formula:C₁₁H₁₂Br₂O₂
Molecular Weight:336.023
Hs Code.:
Mol file:422569-46-8.mol

Synonyms:tert-butyl 3,5-dibromobenzoate

Suppliers and Price of tert-butyl 3,5-dibromobenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
tert-Butyl3,5-dibromobenzoate 95+%
1g
$ 385.00

Alichem
Tert-butyl3,5-dibromobenzoate
250mg
$ 165.64

Alichem
Tert-butyl3,5-dibromobenzoate
1g
$ 401.80

A1 Biochem Labs
tert-Butyl3,5-dibromobenzoate 95%
5 g
$ 650.00

Total 2 raw suppliers

Chemical Property of tert-butyl 3,5-dibromobenzoate

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

tert-Butyl3,5-dibromobenzoate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tert-butyl 3,5-dibromobenzoate

There total 3 articles about tert-butyl 3,5-dibromobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 626-39-1
1,3,5-trisbromobenzene

: 24424-99-5
di-tert-butyl dicarbonate

: 422569-46-8
tert-butyl 3,5-dibromobenzoate

Guidance literature:: 1,3,5-trisbromobenzene; With n-butyllithium; butyl magnesium bromide; In tetrahydrofuran; hexane; toluene; at -10 ℃;

di-tert-butyl dicarbonate; In tetrahydrofuran; hexane; toluene; at -10 ℃;

With citric acid; In tetrahydrofuran; hexane; toluene; Further stages.;
DOI:10.1016/j.tetlet.2007.12.134

Reference yield: 70.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 618-58-6
3,5-dibromobenzoic acid

: 422569-46-8
tert-butyl 3,5-dibromobenzoate

Guidance literature:: With dmap; In tert-butyl alcohol; at 40 ℃; for 13h; Inert atmosphere;
DOI:10.1021/acs.orglett.1c03866

Reference yield:

: 618-58-6
3,5-dibromobenzoic acid

: 75-65-0
tert-butyl alcohol

: 422569-46-8
tert-butyl 3,5-dibromobenzoate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; Cooling with ice;