(1'R,2'S,5'R)-menthyl 3-benzyloxycarbonyl-2-oxaimidazolidine-4(S)-carboxylate

Base Information

Chemical Name:(1'R,2'S,5'R)-menthyl 3-benzyloxycarbonyl-2-oxaimidazolidine-4(S)-carboxylate
CAS No.:865535-05-3
Molecular Formula:C₂₂H₃₀N₂O₅
Molecular Weight:402.491
Hs Code.:

Synonyms:(1'R,2'S,5'R)-menthyl 3-benzyloxycarbonyl-2-oxaimidazolidine-4(S)-carboxylate

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Chemical Property of (1'R,2'S,5'R)-menthyl 3-benzyloxycarbonyl-2-oxaimidazolidine-4(S)-carboxylate

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Technology Process of (1'R,2'S,5'R)-menthyl 3-benzyloxycarbonyl-2-oxaimidazolidine-4(S)-carboxylate

There total 1 articles about (1'R,2'S,5'R)-menthyl 3-benzyloxycarbonyl-2-oxaimidazolidine-4(S)-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 2216-51-5
(-)-menthol

: 59760-01-9,76497-31-9,46961-70-0
(S)-2-oxo-imidazolidine-1,5-dicarboxylic acid 1-benzyl ester

: 865535-05-3
(1'R,2'S,5'R)-menthyl 3-benzyloxycarbonyl-2-oxaimidazolidine-4(S)-carboxylate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 168h;
DOI:10.1002/adsc.200404245

Reference yield: 84.0%

: 75-36-5
acetyl chloride

: 865535-05-3
(1'R,2'S,5'R)-menthyl 3-benzyloxycarbonyl-2-oxaimidazolidine-4(S)-carboxylate

: 865535-06-4
(1'R,2'S,5'R)-menthyl 1-acetyl-3-benzyloxycarbonyl-2-oxaimidazolidine-4(S)-carboxylate

Guidance literature:: With pyridine; dmap; In dichloromethane; Heating;
DOI:10.1002/adsc.200404245

Reference yield:

: 865535-05-3
(1'R,2'S,5'R)-menthyl 3-benzyloxycarbonyl-2-oxaimidazolidine-4(S)-carboxylate

: (1'R,2'S,5'R)-menthyl 1-acetyl-2-oxaimidazolidine-4(S)-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / DMAP; pyridine / CH₂Cl₂ / Heating

2: 78 percent / H₂ / palladium black / ethyl acetate / 760 Torr

With pyridine; dmap; hydrogen; palladium; In dichloromethane; ethyl acetate;
DOI:10.1002/adsc.200404245