N'-(3,5-dichloropyridin-4-yl)bicyclo[2.2.1]hept-5-ene-2-carbohydrazide

Base Information

Chemical Name:N'-(3,5-dichloropyridin-4-yl)bicyclo[2.2.1]hept-5-ene-2-carbohydrazide
CAS No.:1370287-18-5
Molecular Formula:C₁₃H₁₃Cl₂N₃O
Molecular Weight:298.172
Hs Code.:

Synonyms:N'-(3,5-dichloropyridin-4-yl)bicyclo[2.2.1]hept-5-ene-2-carbohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N'-(3,5-dichloropyridin-4-yl)bicyclo[2.2.1]hept-5-ene-2-carbohydrazide

Chemical Property:

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Technology Process of N'-(3,5-dichloropyridin-4-yl)bicyclo[2.2.1]hept-5-ene-2-carbohydrazide

There total 3 articles about N'-(3,5-dichloropyridin-4-yl)bicyclo[2.2.1]hept-5-ene-2-carbohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 934-30-5,1195-12-6,20507-53-3,58001-99-3,67999-50-2,67999-53-5,74645-32-2,108266-75-7,120-74-1
5-norbornene-endo-2-carboxylic acid

: 101620-10-4
4-(4-diphenyl-methyl-1-piperazinyl)butylamine

: 741291-96-3
C₁₆H₁₉NO₄

: C₁₆H₁₇NO₃

: 1370287-18-5
N'-(3,5-dichloropyridin-4-yl)bicyclo[2.2.1]hept-5-ene-2-carbohydrazide

: C₁₆H₂₀O₂

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / Pd/C / ethyl acetate / 1.5 h / 2327.17 Torr

2: 88 percent / DCC; DMAP / CH₂Cl₂ / 3 h / 20 °C

3: KHMDS / tetrahydrofuran; toluene / -78 - 20 °C

With dmap; hydrogen; potassium hexamethylsilazane; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; ethyl acetate; toluene; 3: 3,3-sigmatropic rearrangement;
DOI:10.1021/ol0491888

Reference yield:

: 934-30-5,1195-12-6,20507-53-3,58001-99-3,67999-50-2,67999-53-5,74645-32-2,108266-75-7,120-74-1
5-norbornene-endo-2-carboxylic acid

: 101620-10-4
4-(4-diphenyl-methyl-1-piperazinyl)butylamine

: 741291-96-3
C₁₆H₁₉NO₄

: C₁₆H₁₇NO₃

: 1370287-18-5
N'-(3,5-dichloropyridin-4-yl)bicyclo[2.2.1]hept-5-ene-2-carbohydrazide

: C₁₆H₂₀O₂

: Bicyclo[2.2.1]hept-5-ene-2-carboxylic acid [4-(4-benzhydryl-piperazin-1-yl)-butyl]-amide

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / Pd/C / ethyl acetate / 1.5 h / 2327.17 Torr

2: 88 percent / DCC; DMAP / CH₂Cl₂ / 3 h / 20 °C

3: KHMDS / tetrahydrofuran; toluene / -78 - 20 °C

With dmap; hydrogen; potassium hexamethylsilazane; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; ethyl acetate; toluene; 3: 3,3-sigmatropic rearrangement;
DOI:10.1021/ol0491888

Reference yield:

: 934-30-5,1195-12-6,20507-53-3,58001-99-3,67999-50-2,67999-53-5,74645-32-2,108266-75-7,120-74-1
5-norbornene-endo-2-carboxylic acid

: 101620-10-4
4-(4-diphenyl-methyl-1-piperazinyl)butylamine

: 741291-96-3
C₁₆H₁₉NO₄

: C₁₆H₁₇NO₃

: 1370287-18-5
N'-(3,5-dichloropyridin-4-yl)bicyclo[2.2.1]hept-5-ene-2-carbohydrazide

: C₁₆H₂₀O₂

: Bicyclo[2.2.1]hept-5-ene-2-carboxylic acid [4-(4-benzhydryl-piperazin-1-yl)-butyl]-amide

: exo-1,2,3,4,4a,8b-hexahydro-1,4-methanobiphenylene-2-carboxylic acid

Guidance literature:: With [Cl₂Ru(CHPh)(Cy₂P-(CH₂)15-CH₃)2]; sodium tetraborate buffer; dioleoylphosphatidylcholine; pH=8;
DOI:10.1021/ja045482j