5-(benzotriazol-1-yl-methyl)-3-ethylmercapto-4-phenyl-4H-[1,2,4]triazole

Base Information

Chemical Name:5-(benzotriazol-1-yl-methyl)-3-ethylmercapto-4-phenyl-4H-[1,2,4]triazole
CAS No.:122503-06-4
Molecular Formula:C₁₇H₁₆N₆S
Molecular Weight:336.42
Hs Code.:

Synonyms:5-(benzotriazol-1-yl-methyl)-3-ethylmercapto-4-phenyl-4H-[1,2,4]triazole

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Chemical Property of 5-(benzotriazol-1-yl-methyl)-3-ethylmercapto-4-phenyl-4H-[1,2,4]triazole

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Technology Process of 5-(benzotriazol-1-yl-methyl)-3-ethylmercapto-4-phenyl-4H-[1,2,4]triazole

There total 6 articles about 5-(benzotriazol-1-yl-methyl)-3-ethylmercapto-4-phenyl-4H-[1,2,4]triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 122503-02-0
1-(4-phenyl-4H-1,2,4-triazole-3-thion-5-yl)methyl-1H-benzotriazole

: 75-03-6
ethyl iodide

: 122503-06-4
5-(benzotriazol-1-yl-methyl)-3-ethylmercapto-4-phenyl-4H-[1,2,4]triazole

Guidance literature:: With sodium ethanolate; In ethanol; for 2h; Heating;
DOI:10.1002/jhet.5570260131

Reference yield:

: 69218-46-8
ethyl (1H-benzotriazol-1-yl)acetate

: 122503-06-4
5-(benzotriazol-1-yl-methyl)-3-ethylmercapto-4-phenyl-4H-[1,2,4]triazole

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / hydrazine hydrate / ethanol / 1 h / Heating

2: 75 percent / ethanol / 0.25 h / Heating

3: 95 percent / 5percent aq. sodium hydroxide / 1 h / Heating

4: 90 percent / sodium ethoxide / ethanol / 2 h / Heating

With sodium hydroxide; sodium ethanolate; hydrazine hydrate; In ethanol;
DOI:10.1002/jhet.5570260131

Reference yield:

: 122502-94-7
2-(1H-benzo[d][1,2,3]triazol-1-yl)acetohydrazide

: 122503-06-4
5-(benzotriazol-1-yl-methyl)-3-ethylmercapto-4-phenyl-4H-[1,2,4]triazole

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / ethanol / 0.25 h / Heating

2: 95 percent / 5percent aq. sodium hydroxide / 1 h / Heating

3: 90 percent / sodium ethoxide / ethanol / 2 h / Heating

With sodium hydroxide; sodium ethanolate; In ethanol;
DOI:10.1002/jhet.5570260131