N-(t-butoxycarbonylsulfamoyl)-N-(2-benzyloxy-4-iodophenyl)glycine tert-butyl ester

Base Information

Chemical Name:N-(t-butoxycarbonylsulfamoyl)-N-(2-benzyloxy-4-iodophenyl)glycine tert-butyl ester
CAS No.:1057340-18-7
Molecular Formula:C₂₄H₃₁IN₂O₇S
Molecular Weight:618.49
Hs Code.:

Synonyms:N-(t-butoxycarbonylsulfamoyl)-N-(2-benzyloxy-4-iodophenyl)glycine tert-butyl ester

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Chemical Property of N-(t-butoxycarbonylsulfamoyl)-N-(2-benzyloxy-4-iodophenyl)glycine tert-butyl ester

Chemical Property:

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Technology Process of N-(t-butoxycarbonylsulfamoyl)-N-(2-benzyloxy-4-iodophenyl)glycine tert-butyl ester

There total 5 articles about N-(t-butoxycarbonylsulfamoyl)-N-(2-benzyloxy-4-iodophenyl)glycine tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1189-71-5
isocyanate de chlorosulfonyle

: 1057342-22-9
(2-benzyloxy-4-iodophenylamino)-acetic acid tert-butyl ester

: 75-65-0
tert-butyl alcohol

: 1057340-18-7
N-(t-butoxycarbonylsulfamoyl)-N-(2-benzyloxy-4-iodophenyl)glycine tert-butyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 0.5h;

Reference yield:

: 27783-55-7
5-iodo-2-nitrophenol

: 1057340-18-7
N-(t-butoxycarbonylsulfamoyl)-N-(2-benzyloxy-4-iodophenyl)glycine tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 65 °C

2: iron; acetic acid / ethanol / 1.5 h / 100 °C

3: potassium carbonate / N,N-dimethyl-formamide / 4 h / 50 °C

4: triethylamine / dichloromethane / 0.5 h / 0 °C

With iron; potassium carbonate; acetic acid; triethylamine; In ethanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1057340-17-6
2-benzyloxy-4-iodo-1-nitrobenzene

: 1057340-18-7
N-(t-butoxycarbonylsulfamoyl)-N-(2-benzyloxy-4-iodophenyl)glycine tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: iron; acetic acid / ethanol / 1.5 h / 100 °C

2: potassium carbonate / N,N-dimethyl-formamide / 4 h / 50 °C

3: triethylamine / dichloromethane / 0.5 h / 0 °C

With iron; potassium carbonate; acetic acid; triethylamine; In ethanol; dichloromethane; N,N-dimethyl-formamide;