3-(dimesitylmethoxysilyl)-1,1-dimesityl-2,2-bis(trimethylsilyl)-1-silacyclopropane

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Chemical Name:3-(dimesitylmethoxysilyl)-1,1-dimesityl-2,2-bis(trimethylsilyl)-1-silacyclopropane
CAS No.:99053-98-2
Molecular Formula:C₄₅H₆₆OSi₄
Molecular Weight:735.36
Hs Code.:

Synonyms:3-(dimesitylmethoxysilyl)-1,1-dimesityl-2,2-bis(trimethylsilyl)-1-silacyclopropane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(dimesitylmethoxysilyl)-1,1-dimesityl-2,2-bis(trimethylsilyl)-1-silacyclopropane

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Technology Process of 3-(dimesitylmethoxysilyl)-1,1-dimesityl-2,2-bis(trimethylsilyl)-1-silacyclopropane

There total 5 articles about 3-(dimesitylmethoxysilyl)-1,1-dimesityl-2,2-bis(trimethylsilyl)-1-silacyclopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 67-56-1
methanol

: 99053-94-8
1,1,2,2-tetramesityl-3,4-bis(trimethylsilyl)-1,2-disilacyclobut-3-ene

: 99053-98-2
3-(dimesitylmethoxysilyl)-1,1-dimesityl-2,2-bis(trimethylsilyl)-1-silacyclopropane

Guidance literature:: In cyclohexane; at 120 ℃; for 1h;
DOI:10.1021/ja00311a080

Reference yield: 100.0%

: 67-56-1
methanol

: 83846-02-0
1,1,2,2-tetramesityl-3--1,2-disilacyclopropane

: 99053-98-2
3-(dimesitylmethoxysilyl)-1,1-dimesityl-2,2-bis(trimethylsilyl)-1-silacyclopropane

Guidance literature:: In cyclohexane; at 120 ℃; for 1h;
DOI:10.1021/ja00311a080

Reference yield:

: 5599-27-9
dichloro(dimesityl)silane

: 99053-98-2
3-(dimesitylmethoxysilyl)-1,1-dimesityl-2,2-bis(trimethylsilyl)-1-silacyclopropane

Guidance literature:: Multi-step reaction with 3 steps

1: 51 percent / Na, K / heptane; benzene / 10 h / Heating

2: 25 percent / hexane / 7 h / -40 - -20 °C / Irradiation

3: 100 percent / cyclohexane / 1 h / 120 °C

With sodium; In hexane; n-heptane; cyclohexane; benzene;
DOI:10.1021/ja00311a080