[3-({[4-bromo-1-(2,2-dimethylpropyl)-1H-1,2,3-benzotriazol-5-yl]oxy}methyl)phenyl]boronic acid

Base Information

Chemical Name:[3-({[4-bromo-1-(2,2-dimethylpropyl)-1H-1,2,3-benzotriazol-5-yl]oxy}methyl)phenyl]boronic acid
CAS No.:1379545-29-5
Molecular Formula:C₁₈H₂₁BBrN₃O₃
Molecular Weight:418.098
Hs Code.:

Synonyms:[3-({[4-bromo-1-(2,2-dimethylpropyl)-1H-1,2,3-benzotriazol-5-yl]oxy}methyl)phenyl]boronic acid

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Chemical Property of [3-({[4-bromo-1-(2,2-dimethylpropyl)-1H-1,2,3-benzotriazol-5-yl]oxy}methyl)phenyl]boronic acid

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Technology Process of [3-({[4-bromo-1-(2,2-dimethylpropyl)-1H-1,2,3-benzotriazol-5-yl]oxy}methyl)phenyl]boronic acid

There total 11 articles about [3-({[4-bromo-1-(2,2-dimethylpropyl)-1H-1,2,3-benzotriazol-5-yl]oxy}methyl)phenyl]boronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 908288-77-7
4-bromo-1-(2,2-dimethylpropyl)-1H-1,2,3-benzotriazol-5-ol

: 51323-43-4
(3-(bromomethyl)phenyl)boronic acid

: 1379545-29-5
[3-({[4-bromo-1-(2,2-dimethylpropyl)-1H-1,2,3-benzotriazol-5-yl]oxy}methyl)phenyl]boronic acid

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 369-36-8
6-fluoro-3-nitroaniline

: 1379545-29-5
[3-({[4-bromo-1-(2,2-dimethylpropyl)-1H-1,2,3-benzotriazol-5-yl]oxy}methyl)phenyl]boronic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: dimethyl sulfoxide / 48 h / 120 °C

1.2: 0.33 h / 20 °C

1.3: pH 7

2.1: hydrogen / palladium 10% on activated carbon / ethanol / 5 h / 20 °C / 760.05 Torr / Inert atmosphere

3.1: sodium nitrite; sulfuric acid / water / 0.83 h / 20 - 120 °C / Microwave irradiation

4.1: pyridinium hydrobromide perbromide / chloroform / 20 °C

4.2: pH 7

5.1: caesium carbonate / N,N-dimethyl-formamide / 20 °C

With pyridinium hydrobromide perbromide; sulfuric acid; hydrogen; caesium carbonate; sodium nitrite; palladium 10% on activated carbon; In ethanol; chloroform; water; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 96-96-8
4-methoxy-2-nitroaniline

: 1379545-29-5
[3-({[4-bromo-1-(2,2-dimethylpropyl)-1H-1,2,3-benzotriazol-5-yl]oxy}methyl)phenyl]boronic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: acetic acid; sodium tris(acetoxy)borohydride / dichloromethane / 20 °C

2.1: hydrogen / palladium 10% on activated carbon / ethanol / 20 °C / 760.05 Torr / Inert atmosphere

3.1: sodium nitrite; acetic acid / water / 3 h / 0 - 20 °C

3.3: pH ~ 10

4.1: boron tribromide / dichloromethane / 20 °C

4.2: pH 7

5.1: caesium carbonate / N,N-dimethyl-formamide / 20 °C

With hydrogen; boron tribromide; sodium tris(acetoxy)borohydride; caesium carbonate; acetic acid; sodium nitrite; palladium 10% on activated carbon; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;