(R)-(+)-3-<4-<2-(cyclopropylmethoxy)ethyl>phenoxy>-1,2-propanodiol acetonide

Base Information

Chemical Name:(R)-(+)-3-<4-<2-(cyclopropylmethoxy)ethyl>phenoxy>-1,2-propanodiol acetonide
CAS No.:108008-05-5
Molecular Formula:C₁₈H₂₆O₄
Molecular Weight:306.402
Hs Code.:

Synonyms:(R)-(+)-3-<4-<2-(cyclopropylmethoxy)ethyl>phenoxy>-1,2-propanodiol acetonide

Suppliers and Price of (R)-(+)-3-<4-<2-(cyclopropylmethoxy)ethyl>phenoxy>-1,2-propanodiol acetonide

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Chemical Property of (R)-(+)-3-<4-<2-(cyclopropylmethoxy)ethyl>phenoxy>-1,2-propanodiol acetonide

Chemical Property:

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Technology Process of (R)-(+)-3-<4-<2-(cyclopropylmethoxy)ethyl>phenoxy>-1,2-propanodiol acetonide

There total 4 articles about (R)-(+)-3-<4-<2-(cyclopropylmethoxy)ethyl>phenoxy>-1,2-propanodiol acetonide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 63659-15-4
1-benzyloxy-4-(2-cyclopropylmethoxyethyl)benzene

: 108008-05-5
(R)-(+)-3-<4-<2-(cyclopropylmethoxy)ethyl>phenoxy>-1,2-propanodiol acetonide

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / H₂ / 5percent Pd/C / tetrahydrofuran / 50 - 60 °C / 2585.7 Torr

2: NaOH / ethanol / 24 h / Heating

With sodium hydroxide; hydrogen; palladium on activated charcoal; In tetrahydrofuran; ethanol;
DOI:10.1021/jm00389a008

Reference yield:

: 61439-59-6
2-(4-benzyloxyphenyl)ethanol

: 108008-05-5
(R)-(+)-3-<4-<2-(cyclopropylmethoxy)ethyl>phenoxy>-1,2-propanodiol acetonide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1.) DMF, 2.) DMF, 60 deg, 18 h

2: 84 percent / H₂ / 5percent Pd/C / tetrahydrofuran / 50 - 60 °C / 2585.7 Torr

3: NaOH / ethanol / 24 h / Heating

With sodium hydroxide; hydrogen; sodium hydride; palladium on activated charcoal; In tetrahydrofuran; ethanol;
DOI:10.1021/jm00389a008

Reference yield:

: 56441-69-1
2-<4-(phenylmethoxy)phenyl>acetic acid ethyl ester

: 108008-05-5
(R)-(+)-3-<4-<2-(cyclopropylmethoxy)ethyl>phenoxy>-1,2-propanodiol acetonide

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / LiAlH₄ / tetrahydrofuran / 3 h / Ambient temperature

2: 1.) NaH / 1.) DMF, 2.) DMF, 60 deg, 18 h

3: 84 percent / H₂ / 5percent Pd/C / tetrahydrofuran / 50 - 60 °C / 2585.7 Torr

4: NaOH / ethanol / 24 h / Heating

With sodium hydroxide; lithium aluminium tetrahydride; hydrogen; sodium hydride; palladium on activated charcoal; In tetrahydrofuran; ethanol;
DOI:10.1021/jm00389a008