C₃₅H₃₄BrCl₃N₂O₁₁S

Base Information

Chemical Name:C₃₅H₃₄BrCl₃N₂O₁₁S
CAS No.:1234550-72-1
Molecular Formula:C₃₅H₃₄BrCl₃N₂O₁₁S
Molecular Weight:876.991
Hs Code.:

C<sub>35</sub>H<sub>34</sub>BrCl<sub>3</sub>N<sub>2</sub>O<sub>11</sub>S

Synonyms:C₃₅H₃₄BrCl₃N₂O₁₁S

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Chemical Property of C₃₅H₃₄BrCl₃N₂O₁₁S

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Technology Process of C₃₅H₃₄BrCl₃N₂O₁₁S

There total 21 articles about C₃₅H₃₄BrCl₃N₂O₁₁S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1234550-73-2
(S)-2,2,2-trichloroethyl 4-((R)-2-(benzyloxy)-1-(7-methyl-6-(methylsulfonyloxy)benzo[d][1,3]dioxol-4-yl)ethyl)-2-(2-bromo-5-hydroxy-4-methoxy-3-methylbenzyl)-5-methyl-3-oxo-3,4-dihydropyrazine-1(2H)-carboxylate

: 1234550-72-1
C₃₅H₃₄BrCl₃N₂O₁₁S

Guidance literature:: With phenyltrimethylammonium tribromide; In acetonitrile; at 20 - 60 ℃; Inert atmosphere; Molecular sieve;
DOI:10.1021/jo100788j

Reference yield:

: 1177255-35-4
(S)-methyl 3-(2-bromo-5-hydroxy-4-methoxy-3-methylphenyl)-2-(tert-butoxycarbonylamino)propanoate

: 1234550-72-1
C₃₅H₃₄BrCl₃N₂O₁₁S

Guidance literature:: Multi-step reaction with 10 steps

1.1: tetra-(n-butyl)ammonium iodide; potassium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

2.1: methanol; acetyl chloride / dichloromethane / 5 h / 20 °C / Inert atmosphere

3.1: lithium hydroxide monohydrate / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere; Molecular sieve

3.2: 20 h / 20 °C / Inert atmosphere; Molecular sieve

4.1: sodium hydrogencarbonate / dichloromethane; water / 2 h / 0 °C

5.1: tin(II) bromide / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere

6.1: lithium hydroxide / tetrahydrofuran; methanol; water / 0 - 20 °C

6.2: 0 °C

7.1: (triphenylphosphine)gold(I) chloride; silver(I) triflimide / dichloromethane / 3.5 h / 20 °C / Inert atmosphere

8.1: dichloromethane / 22 h / 20 °C / Inert atmosphere

9.1: magnesium sulfate; toluene-4-sulfonic acid / toluene / 12 h / 90 °C / Inert atmosphere

10.1: phenyltrimethylammonium tribromide / acetonitrile / 20 - 60 °C / Inert atmosphere; Molecular sieve

With methanol; (triphenylphosphine)gold(I) chloride; lithium hydroxide monohydrate; tetra-(n-butyl)ammonium iodide; phenyltrimethylammonium tribromide; tin(II) bromide; sodium hydrogencarbonate; magnesium sulfate; potassium carbonate; toluene-4-sulfonic acid; acetyl chloride; lithium hydroxide; silver(I) triflimide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; 10.1: Friedel Crafts alkylation;
DOI:10.1021/jo100788j

Reference yield:

: 1150635-60-1
C₂₂H₂₅NO₇

: 1234550-72-1
C₃₅H₃₄BrCl₃N₂O₁₁S

Guidance literature:: Multi-step reaction with 13 steps

1.1: methanol; potassium carbonate / 1 h / 0 °C / Inert atmosphere

1.2: 0 °C / pH 3

2.1: 10% palladium on activated carbon; hydrogen / methanol / 10 h / 20 °C / 760.05 Torr

3.1: N-Bromosuccinimide / acetonitrile / 1 h / 0 °C / Inert atmosphere

4.1: tetra-(n-butyl)ammonium iodide; potassium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

5.1: methanol; acetyl chloride / dichloromethane / 5 h / 20 °C / Inert atmosphere

6.1: lithium hydroxide monohydrate / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere; Molecular sieve

6.2: 20 h / 20 °C / Inert atmosphere; Molecular sieve

7.1: sodium hydrogencarbonate / dichloromethane; water / 2 h / 0 °C

8.1: tin(II) bromide / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere

9.1: lithium hydroxide / tetrahydrofuran; methanol; water / 0 - 20 °C

9.2: 0 °C

10.1: (triphenylphosphine)gold(I) chloride; silver(I) triflimide / dichloromethane / 3.5 h / 20 °C / Inert atmosphere

11.1: dichloromethane / 22 h / 20 °C / Inert atmosphere

12.1: magnesium sulfate; toluene-4-sulfonic acid / toluene / 12 h / 90 °C / Inert atmosphere

13.1: phenyltrimethylammonium tribromide / acetonitrile / 20 - 60 °C / Inert atmosphere; Molecular sieve

With methanol; N-Bromosuccinimide; (triphenylphosphine)gold(I) chloride; lithium hydroxide monohydrate; 10% palladium on activated carbon; hydrogen; tetra-(n-butyl)ammonium iodide; phenyltrimethylammonium tribromide; tin(II) bromide; sodium hydrogencarbonate; magnesium sulfate; potassium carbonate; toluene-4-sulfonic acid; acetyl chloride; lithium hydroxide; silver(I) triflimide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; 13.1: Friedel Crafts alkylation;
DOI:10.1021/jo100788j