benzyl-[3-(benzyl-ethoxycarbonyl-amino)-2-oxo-3-phenylsulfanyl-propyl]-carbamic acid ethyl ester

Base Information

Chemical Name:benzyl-[3-(benzyl-ethoxycarbonyl-amino)-2-oxo-3-phenylsulfanyl-propyl]-carbamic acid ethyl ester
CAS No.:253590-95-3
Molecular Formula:C₂₉H₃₂N₂O₅S
Molecular Weight:520.649
Hs Code.:

Synonyms:benzyl-[3-(benzyl-ethoxycarbonyl-amino)-2-oxo-3-phenylsulfanyl-propyl]-carbamic acid ethyl ester

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Chemical Property of benzyl-[3-(benzyl-ethoxycarbonyl-amino)-2-oxo-3-phenylsulfanyl-propyl]-carbamic acid ethyl ester

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Technology Process of benzyl-[3-(benzyl-ethoxycarbonyl-amino)-2-oxo-3-phenylsulfanyl-propyl]-carbamic acid ethyl ester

There total 5 articles about benzyl-[3-(benzyl-ethoxycarbonyl-amino)-2-oxo-3-phenylsulfanyl-propyl]-carbamic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1212-08-4
S-Phenyl benzenethiosulfonate

: 253590-76-0
benzyl-[3-(benzyl-ethoxycarbonyl-amino)-2-oxo-propyl]-carbamic acid ethyl ester

: 253590-95-3
benzyl-[3-(benzyl-ethoxycarbonyl-amino)-2-oxo-3-phenylsulfanyl-propyl]-carbamic acid ethyl ester

Guidance literature:: With n-butyllithium; In 1,2-dichloro-ethane; at -25 - 20 ℃; for 1h;
DOI:10.1016/S0223-5234(00)80031-8

Reference yield:

: 100-52-7
benzaldehyde

: 253590-95-3
benzyl-[3-(benzyl-ethoxycarbonyl-amino)-2-oxo-3-phenylsulfanyl-propyl]-carbamic acid ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: Na₂SO₄ / CH₂Cl₂ / 20 °C

2: NaBH₄ / ethanol / 20 °C

3: 100 percent / Et₃N / CH₂Cl₂ / 1 h / 0 - 20 °C

4: 93 percent / NaOCl; sat. NaHCO₃; KBr / TEMPO / CH₂Cl₂; H₂O / 0 - 20 °C

5: 45 percent / nBuLi / 1,2-dichloro-ethane / 1 h / -25 - 20 °C

With sodium hypochlorite; sodium tetrahydroborate; n-butyllithium; sodium hydrogencarbonate; sodium sulfate; triethylamine; potassium bromide; 2,2,6,6-tetramethyl-piperidine-N-oxyl; In ethanol; dichloromethane; water; 1,2-dichloro-ethane; 1: Condensation / 2: Reduction / 3: Carboxylation / 4: Oxidation / 5: Substitution;
DOI:10.1016/S0223-5234(00)80031-8

Reference yield:

: 65838-17-7
1,3-di-(N-benzylamino)-2-hydroxypropane

: 253590-95-3
benzyl-[3-(benzyl-ethoxycarbonyl-amino)-2-oxo-3-phenylsulfanyl-propyl]-carbamic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / Et₃N / CH₂Cl₂ / 1 h / 0 - 20 °C

2: 93 percent / NaOCl; sat. NaHCO₃; KBr / TEMPO / CH₂Cl₂; H₂O / 0 - 20 °C

3: 45 percent / nBuLi / 1,2-dichloro-ethane / 1 h / -25 - 20 °C

With sodium hypochlorite; n-butyllithium; sodium hydrogencarbonate; triethylamine; potassium bromide; 2,2,6,6-tetramethyl-piperidine-N-oxyl; In dichloromethane; water; 1,2-dichloro-ethane; 1: Carboxylation / 2: Oxidation / 3: Substitution;
DOI:10.1016/S0223-5234(00)80031-8