(S(S),2S,3S,1'S)-N-(tert-butylsulfinyl)-2-(1-amino-3-phenylpropyl)-3-methylcyclohexanone

Base Information

Chemical Name:(S(S),2S,3S,1'S)-N-(tert-butylsulfinyl)-2-(1-amino-3-phenylpropyl)-3-methylcyclohexanone
CAS No.:1126903-68-1
Molecular Formula:C₂₀H₃₁NO₂S
Molecular Weight:349.538
Hs Code.:

Synonyms:(S(S),2S,3S,1'S)-N-(tert-butylsulfinyl)-2-(1-amino-3-phenylpropyl)-3-methylcyclohexanone

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Chemical Property of (S(S),2S,3S,1'S)-N-(tert-butylsulfinyl)-2-(1-amino-3-phenylpropyl)-3-methylcyclohexanone

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Technology Process of (S(S),2S,3S,1'S)-N-(tert-butylsulfinyl)-2-(1-amino-3-phenylpropyl)-3-methylcyclohexanone

There total 1 articles about (S(S),2S,3S,1'S)-N-(tert-butylsulfinyl)-2-(1-amino-3-phenylpropyl)-3-methylcyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 930-68-7
cyclohexenone

: 1190958-35-0
(S)-2-methyl-N-(3-phenylpropylidene)propane-2-sulfinamide

: 544-97-8
dimethyl zinc(II)

: 1126903-68-1
(S(S),2S,3S,1'S)-N-(tert-butylsulfinyl)-2-(1-amino-3-phenylpropyl)-3-methylcyclohexanone

Guidance literature:: cyclohexenone; (S)-2-methyl-N-(3-phenylpropylidene)propane-2-sulfinamide; With (S)-(+)-(3,5-dioxa-4-phosphacyclohepta[2,1-a;3,4-a']dinaphthalen-4-yl)-bis-[(1R)-1-phenethyl]amine; copper(II) bis(trifluoromethanesulfonate); In dichloromethane; at 20 ℃; for 0.25h; Inert atmosphere;

dimethyl zinc(II); In dichloromethane; toluene; at -40 - -20 ℃; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/jo802812w

Reference yield: 70.0%

: 1126903-68-1
(S(S),2S,3S,1'S)-N-(tert-butylsulfinyl)-2-(1-amino-3-phenylpropyl)-3-methylcyclohexanone

: 1126904-02-6
(6S,7S,1'S)-N-(tert-butylsulfonyl)-7-(1-amino-3-phenylpropyl)-6-methyloxepan-2-one

Guidance literature:: (S(S),2S,3S,1'S)-N-(tert-butylsulfinyl)-2-(1-amino-3-phenylpropyl)-3-methylcyclohexanone; With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 5 ℃; for 0.5h;

With sodium hydrogencarbonate; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1021/jo802812w