{Pd₂Co₂(CO)7(dppm)2}

Base Information

Chemical Name:{Pd₂Co₂(CO)7(dppm)2}
CAS No.:113109-24-3
Molecular Formula:C₅₇H₄₄Co₂O₇P₄Pd₂
Molecular Weight:1295.69
Hs Code.:

{Pd<sub>2</sub>Co<sub>2</sub>(CO)7(dppm)2}

Synonyms:{Pd₂Co₂(CO)7(dppm)2}

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Chemical Property of {Pd₂Co₂(CO)7(dppm)2}

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Technology Process of {Pd₂Co₂(CO)7(dppm)2}

There total 4 articles about {Pd₂Co₂(CO)7(dppm)2} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 14878-28-5
sodium tetracarbonyl cobaltate

: 64345-29-5
Pd2Cl2(μ-bis(diphenylphosphino)methane)2

: 113109-24-3
{Pd₂Co₂(CO)7(dppm)2}

: 64345-32-0
Pd2(μ-CO)Cl2(μ-dppm)2

Guidance literature:: In tetrahydrofuran; byproducts: NaCl; A filtered soln. of Na{Co(CO)4} in THF was added to a cooled (-78°C) and stirred suspn. of Pd2Cl2(dppm)2 in THF. The react. temp. was raised to 0°C (3h) and then to 20°C (5h).; The mixt. was filtered to remove insol. NaCl and Pd2Cl2(μ-CO)(dppm)2. Addn. of n-hexane gave, after cooling at -20°C, a powder, which was washed with H2O, dried in vac. and recrystd. from CH2Cl2/n-hexane. Elem.anal.;

Reference yield: 66.0%

: 14878-28-5
sodium tetracarbonyl cobaltate

: 64345-32-0
Pd2(μ-CO)Cl2(μ-dppm)2

: 113109-24-3
{Pd₂Co₂(CO)7(dppm)2}

Guidance literature:: In tetrahydrofuran; A filtered soln. of Na{Co(CO)4} in THF was added to a cooled (-78°C) susp. of {Pd2Cl2(μ-CO)(dppm)2} in THF. The temp. was raised to 20°C. The stirring was maintained for 4 ds.; The mixt. was filtered. Addn. of n-hexane gave, after cooling at -20°C, a powder, which was washed with water, dried in vac., and recrystd. from CH2Cl2/n-hexane. Unreacted {Pd2Cl2(μ-CO)(dppm)2} (29%);

Reference yield: 10.0%

: 14878-28-5
sodium tetracarbonyl cobaltate

: 78274-94-9
{Pd2Cl2(μ-CH2)(dppm)2}*0.25CH2Cl2

: 113109-24-3
{Pd₂Co₂(CO)7(dppm)2}

Guidance literature:: In diethyl ether; Solid Na{Co(CO)4} was added to a susp. of {Pd2Cl2(μ-CH2)(dppm)2} in Et2O. Stirring was maintained for 20 h.; The mixt. was evapd. to dryness, and the residue was extd. with toluene and filtered and the solvent evapd. in vac.;