2-methylene-4-<(4-methylphenylsulfonyl)methyl>decanoic acid methyl ester

Base Information

Chemical Name:2-methylene-4-<(4-methylphenylsulfonyl)methyl>decanoic acid methyl ester
CAS No.:129222-61-3
Molecular Formula:C₂₀H₃₀O₄S
Molecular Weight:366.522
Hs Code.:

Synonyms:2-methylene-4-<(4-methylphenylsulfonyl)methyl>decanoic acid methyl ester

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Chemical Property of 2-methylene-4-<(4-methylphenylsulfonyl)methyl>decanoic acid methyl ester

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Technology Process of 2-methylene-4-<(4-methylphenylsulfonyl)methyl>decanoic acid methyl ester

There total 3 articles about 2-methylene-4-<(4-methylphenylsulfonyl)methyl>decanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 111-66-0,25068-25-1
oct-1-ene

: 126234-89-7
2-<(4-methylphenylsulfonyl)methyl>propenoic acid methyl ester

: 129222-61-3
2-methylene-4-<(4-methylphenylsulfonyl)methyl>decanoic acid methyl ester

Guidance literature:: With dibenzoyl peroxide; In tetrachloromethane; for 12h; Heating;
DOI:10.1016/S0040-4020(97)00306-2

Reference yield:

: 1950-78-3
p-toluenesulfonyl iodide

: 129222-61-3
2-methylene-4-<(4-methylphenylsulfonyl)methyl>decanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) Et₃N / 1.) CCl₄, 20 deg C, light, 2.) CCl₄, reflux, 15 h

2: 63 percent / benzoyl peroxide / CCl₄ / 12 h / Heating

With triethylamine; dibenzoyl peroxide; In tetrachloromethane;
DOI:10.1016/S0040-4020(97)00306-2

Reference yield:

: 824-79-3
sodium 4-methylbenzenesulfinate

: 129222-61-3
2-methylene-4-<(4-methylphenylsulfonyl)methyl>decanoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: I₂ / ethanol; H₂O

2: 2.) Et₃N / 1.) CCl₄, 20 deg C, light, 2.) CCl₄, reflux, 15 h

3: 63 percent / benzoyl peroxide / CCl₄ / 12 h / Heating

With iodine; triethylamine; dibenzoyl peroxide; In tetrachloromethane; ethanol; water;
DOI:10.1016/S0040-4020(97)00306-2