C₂₆H₄₀O₆

Base Information

Chemical Name:C₂₆H₄₀O₆
CAS No.:213026-16-5
Molecular Formula:C₂₆H₄₀O₆
Molecular Weight:448.6
Hs Code.:

C<sub>26</sub>H<sub>40</sub>O<sub>6</sub>

Synonyms:C₂₆H₄₀O₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₆H₄₀O₆

Chemical Property:

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Technology Process of C₂₆H₄₀O₆

There total 12 articles about C₂₆H₄₀O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 213026-15-4
(1R,4aS)-trans-decahydro-1-α-[(2,3,5,6-tetramethoxyphenyl)methyl]-1β,4aβ-dimethyl-2-methylene-5-(2-methyl-1,3-dioxolan-2-yl)-naphthalene

: C₂₆H₄₀O₆

: 213026-16-5
C₂₆H₄₀O₆

Guidance literature:: With methanol; hydrogen; palladium on activated charcoal; In triethylamine; at 20 ℃; for 12h; under 760 Torr;
DOI:10.1021/jo9805192

Reference yield:

: 26742-33-6
(4aS)-1,4aβ-dimethyl-4,4a,7,8-tetrahydronaphthalene-2,5(3H,6H)-dione-5-ethyeneacetal

: 213026-16-5
C₂₆H₄₀O₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: 90 percent / Li; H₂O / tetrahydrofuran; liquid ammonia / 1.5 h / -78 - 30 °C

2.1: LDA / hexane; tetrahydrofuran / 1 h / -78 °C

2.2: hexane; tetrahydrofuran / -78 - 20 °C

3.1: 897 mg / Pd(OAc)2 / acetonitrile / 1 h / Heating

4.1: LiHMDS / tetrahydrofuran; hexane / 0.5 h / -78 - 0 °C

4.2: 91 percent / tetrahydrofuran; hexane / 1.5 h / -78 - 50 °C

5.1: 96 percent / hydrogen / Pd/C / ethanol / 4 h / 20 °C / 760 Torr

6.1: NaH / dimethylsulfoxide / 1 h / 0 - 20 °C

6.2: 91 percent / dimethylsulfoxide / 24 h / 75 - 80 °C

7.1: 81 percent / hydrogen; MeOH / Pd/C / triethylamine / 12 h / 20 °C / 760 Torr

With methanol; palladium diacetate; water; hydrogen; lithium; sodium hydride; lithium hexamethyldisilazane; lithium diisopropyl amide; palladium on activated charcoal; In tetrahydrofuran; ethanol; hexane; ammonia; dimethyl sulfoxide; triethylamine; acetonitrile; 1.1: Reduction / 2.1: Metallation / 2.2: silylation / 3.1: Elimination / 4.1: Metallation / 4.2: Alkylation / 5.1: Catalytic hydrogenation / 6.1: Dehydroiodination / 6.2: Wittig olefination / 7.1: Catalytic hydrogenation;
DOI:10.1021/jo9805192

Reference yield:

: 213026-08-5
(4aS,5S,8aS)-(-)-3,4,4a,5,8,8a-Hexahydro-5,8a-dimethylnaphthalene-1(2H),6(7H)-dione 1-ethylene ketal

: 213026-16-5
C₂₆H₄₀O₆

Guidance literature:: Multi-step reaction with 6 steps

1.1: LDA / hexane; tetrahydrofuran / 1 h / -78 °C

1.2: hexane; tetrahydrofuran / -78 - 20 °C

2.1: 897 mg / Pd(OAc)2 / acetonitrile / 1 h / Heating

3.1: LiHMDS / tetrahydrofuran; hexane / 0.5 h / -78 - 0 °C

3.2: 91 percent / tetrahydrofuran; hexane / 1.5 h / -78 - 50 °C

4.1: 96 percent / hydrogen / Pd/C / ethanol / 4 h / 20 °C / 760 Torr

5.1: NaH / dimethylsulfoxide / 1 h / 0 - 20 °C

5.2: 91 percent / dimethylsulfoxide / 24 h / 75 - 80 °C

6.1: 81 percent / hydrogen; MeOH / Pd/C / triethylamine / 12 h / 20 °C / 760 Torr

With methanol; palladium diacetate; hydrogen; sodium hydride; lithium hexamethyldisilazane; lithium diisopropyl amide; palladium on activated charcoal; In tetrahydrofuran; ethanol; hexane; dimethyl sulfoxide; triethylamine; acetonitrile; 1.1: Metallation / 1.2: silylation / 2.1: Elimination / 3.1: Metallation / 3.2: Alkylation / 4.1: Catalytic hydrogenation / 5.1: Dehydroiodination / 5.2: Wittig olefination / 6.1: Catalytic hydrogenation;
DOI:10.1021/jo9805192