1,21-phthalimido-5,9,13,17-tetrakis(p-tolylsulfonyl)-1,5,9,13,17,21-hexaazahenicosane

Base Information

Chemical Name:1,21-phthalimido-5,9,13,17-tetrakis(p-tolylsulfonyl)-1,5,9,13,17,21-hexaazahenicosane
CAS No.:916444-04-7
Molecular Formula:C₅₉H₆₆N₆O₁₂S₄
Molecular Weight:1179.47
Hs Code.:

Synonyms:1,21-phthalimido-5,9,13,17-tetrakis(p-tolylsulfonyl)-1,5,9,13,17,21-hexaazahenicosane

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Chemical Property of 1,21-phthalimido-5,9,13,17-tetrakis(p-tolylsulfonyl)-1,5,9,13,17,21-hexaazahenicosane

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Technology Process of 1,21-phthalimido-5,9,13,17-tetrakis(p-tolylsulfonyl)-1,5,9,13,17,21-hexaazahenicosane

There total 3 articles about 1,21-phthalimido-5,9,13,17-tetrakis(p-tolylsulfonyl)-1,5,9,13,17,21-hexaazahenicosane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 5460-29-7
2-(3-bromopropyl)isoindole-1,3-dione

: 67341-38-2
N,N'-bis<3-(tosylamino)propyl>-N,N'-ditosyl-1,3-propanediamine

: 916444-04-7
1,21-phthalimido-5,9,13,17-tetrakis(p-tolylsulfonyl)-1,5,9,13,17,21-hexaazahenicosane

Guidance literature:: With potassium carbonate; In acetonitrile; for 12h; Heating;
DOI:10.1039/b611031b

Reference yield:

: 4605-14-5
N,N'-bis-(3-aminopropyl)-1,3-propanediamine

: 916444-04-7
1,21-phthalimido-5,9,13,17-tetrakis(p-tolylsulfonyl)-1,5,9,13,17,21-hexaazahenicosane

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / water; tetrahydrofuran / 24 h

2: potassium carbonate / acetonitrile / 48 h / Reflux

With potassium carbonate; In tetrahydrofuran; water; acetonitrile;
DOI:10.1039/c3dt51012c

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 916444-04-7
1,21-phthalimido-5,9,13,17-tetrakis(p-tolylsulfonyl)-1,5,9,13,17,21-hexaazahenicosane

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / water; tetrahydrofuran / 24 h

2: potassium carbonate / acetonitrile / 48 h / Reflux

With potassium carbonate; In tetrahydrofuran; water; acetonitrile;
DOI:10.1039/c3dt51012c