N,N',4,8,12,16-hexa(p-toluenesulfonyl)-4,8,12,16-tetraazaundecane-1,19-diamine

Base Information

Chemical Name:N,N',4,8,12,16-hexa(p-toluenesulfonyl)-4,8,12,16-tetraazaundecane-1,19-diamine
CAS No.:87265-96-1
Molecular Formula:C₅₇H₇₄N₆O₁₂S₆
Molecular Weight:1227.64
Hs Code.:

Synonyms:N,N',4,8,12,16-hexa(p-toluenesulfonyl)-4,8,12,16-tetraazaundecane-1,19-diamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N',4,8,12,16-hexa(p-toluenesulfonyl)-4,8,12,16-tetraazaundecane-1,19-diamine

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Technology Process of N,N',4,8,12,16-hexa(p-toluenesulfonyl)-4,8,12,16-tetraazaundecane-1,19-diamine

There total 10 articles about N,N',4,8,12,16-hexa(p-toluenesulfonyl)-4,8,12,16-tetraazaundecane-1,19-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 98-59-9
p-toluenesulfonyl chloride

: 87265-95-0
4,8,12,16-tetra(p-toluenesulfonyl)-4,8,12,16-tetraazaundecane-1,19-diamine

: 87265-96-1
N,N',4,8,12,16-hexa(p-toluenesulfonyl)-4,8,12,16-tetraazaundecane-1,19-diamine

Guidance literature:: With triethylamine; In tetrahydrofuran; for 40h;
DOI:10.1002/hlca.19830660426

Reference yield:

: 67341-38-2
N,N'-bis<3-(tosylamino)propyl>-N,N'-ditosyl-1,3-propanediamine

: 87265-96-1
N,N',4,8,12,16-hexa(p-toluenesulfonyl)-4,8,12,16-tetraazaundecane-1,19-diamine

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / K₂CO₃ / acetonitrile / 12 h / Heating

2: 99 percent / hydrazine monohydrate / tetrahydrofuran / 12 h / Heating

3: 82 percent / pyridine / 10 - 20 °C

With potassium carbonate; hydrazine hydrate; In tetrahydrofuran; pyridine; acetonitrile;
DOI:10.1039/b611031b

Reference yield:

: 916444-04-7
1,21-phthalimido-5,9,13,17-tetrakis(p-tolylsulfonyl)-1,5,9,13,17,21-hexaazahenicosane

: 87265-96-1
N,N',4,8,12,16-hexa(p-toluenesulfonyl)-4,8,12,16-tetraazaundecane-1,19-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / hydrazine monohydrate / tetrahydrofuran / 12 h / Heating

2: 82 percent / pyridine / 10 - 20 °C

With hydrazine hydrate; In tetrahydrofuran; pyridine;
DOI:10.1039/b611031b