3,13,15-tri-O-(S-methyl)thiocarbonyljesaconitine

Base Information

• Chemical Name: 3,13,15-tri-O-(S-methyl)thiocarbonyljesaconitine
• CAS No.: 139617-08-6
• Molecular Formula: C₄₁H₅₅NO₁₂S₆
• Molecular Weight: 946.283
• Mol file: 139617-08-6.mol

Synonyms:3,13,15-tri-O-(S-methyl)thiocarbonyljesaconitine

Chemical Property of 3,13,15-tri-O-(S-methyl)thiocarbonyljesaconitine

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 3,13,15-tri-O-(S-methyl)thiocarbonyljesaconitine

There total 1 articles about 3,13,15-tri-O-(S-methyl)thiocarbonyljesaconitine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

carbon disulfide (75-15-0,12122-00-8) + jesaconitine (16298-90-1) + methyl iodide (74-88-4) → 3,13,15-tri-O-(S-methyl)thiocarbonyljesaconitine (139617-08-6)

Guidance literature:

With 1H-imidazole; sodium hydride; Yield given. Multistep reaction; 1) THF, 0 deg C, 30 min, 2) 1.5h, reflux;

DOI:10.1248/cpb.39.2803

Reference yield: 88.0%

3,13,15-tri-O-(S-methyl)thiocarbonyljesaconitine (139617-08-6) → 3,13,15-trideoxyjesaconitine (73870-35-6)

Guidance literature:

With tri-n-butyl-tin hydride; In benzene; for 4h; Heating;

DOI:10.1248/cpb.39.2803

upstream raw materials:

carbon disulfide

jesaconitine

methyl iodide

Downstream raw materials:

3,13,15-trideoxyjesaconitine

Refernces