C₂₁H₃₁N₅O₅SSi

Base Information

Chemical Name:C₂₁H₃₁N₅O₅SSi
CAS No.:1539304-15-8
Molecular Formula:C₂₁H₃₁N₅O₅SSi
Molecular Weight:493.659
Hs Code.:

C<sub>21</sub>H<sub>31</sub>N<sub>5</sub>O<sub>5</sub>SSi

Synonyms:C₂₁H₃₁N₅O₅SSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₁H₃₁N₅O₅SSi

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Technology Process of C₂₁H₃₁N₅O₅SSi

There total 6 articles about C₂₁H₃₁N₅O₅SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1539304-14-7
ethyl 3-((tert-butyldimethylsilyl)oxy)benzyl(6-chloro-2-(methylthio)-5-nitropyrimidin-4-yl)carbamate

: 1539304-15-8
C₂₁H₃₁N₅O₅SSi

Guidance literature:: With ammonium hydroxide; In tetrahydrofuran; at 20 ℃; for 16h;

Reference yield:

: 1979-98-2
4,6-dihydroxy-2-methylmercaptopyrimidine

: 1539304-15-8
C₂₁H₃₁N₅O₅SSi

Guidance literature:: Multi-step reaction with 6 steps

1.1: trifluoroacetic acid / 0.5 h / 20 °C

1.2: 5 - 20 °C

2.1: trichlorophosphate; N,N-dimethyl-aniline / 2 h / 0 - 100 °C

3.1: triethylamine; ammonia / tetrahydrofuran; isopropyl alcohol / 5 h / 20 °C

4.1: triethylamine / tetrahydrofuran / 6 h / 20 °C

5.1: potassium carbonate; sodium iodide / acetone / 16 h / 20 °C

6.1: ammonium hydroxide / tetrahydrofuran / 16 h / 20 °C

With ammonium hydroxide; ammonia; potassium carbonate; N,N-dimethyl-aniline; triethylamine; trifluoroacetic acid; sodium iodide; trichlorophosphate; In tetrahydrofuran; isopropyl alcohol; acetone;

Reference yield:

: 1979-97-1
2-(methylthio)-5-nitropyrimidine-4,6-diol

: 1539304-15-8
C₂₁H₃₁N₅O₅SSi

Guidance literature:: Multi-step reaction with 5 steps

1: trichlorophosphate; N,N-dimethyl-aniline / 2 h / 0 - 100 °C

2: triethylamine; ammonia / tetrahydrofuran; isopropyl alcohol / 5 h / 20 °C

3: triethylamine / tetrahydrofuran / 6 h / 20 °C

4: potassium carbonate; sodium iodide / acetone / 16 h / 20 °C

5: ammonium hydroxide / tetrahydrofuran / 16 h / 20 °C

With ammonium hydroxide; ammonia; potassium carbonate; N,N-dimethyl-aniline; triethylamine; sodium iodide; trichlorophosphate; In tetrahydrofuran; isopropyl alcohol; acetone;