trans-ethyl 1-ethyl-4-(tert-butyldimethylsilyloxy)-cyclohexanecarboxylate

Base Information

Chemical Name:trans-ethyl 1-ethyl-4-(tert-butyldimethylsilyloxy)-cyclohexanecarboxylate
CAS No.:950772-73-3
Molecular Formula:C₁₇H₃₄O₃Si
Molecular Weight:314.541
Hs Code.:

Synonyms:trans-ethyl 1-ethyl-4-(tert-butyldimethylsilyloxy)-cyclohexanecarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-ethyl 1-ethyl-4-(tert-butyldimethylsilyloxy)-cyclohexanecarboxylate

Chemical Property:

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Technology Process of trans-ethyl 1-ethyl-4-(tert-butyldimethylsilyloxy)-cyclohexanecarboxylate

There total 4 articles about trans-ethyl 1-ethyl-4-(tert-butyldimethylsilyloxy)-cyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 950772-72-2
trans-1-ethyl-4-hydroxy-cyclohexanecarboxylic acid ethyl ester

: 18162-48-6
tert-butyldimethylsilyl chloride

: 950772-73-3
trans-ethyl 1-ethyl-4-(tert-butyldimethylsilyloxy)-cyclohexanecarboxylate

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 862728-40-3
4-(tert-butyl-dimethyl-silyloxy)-1-ethyl-cyclohexanecarboxylic acid ethyl ester

: 950772-73-3
trans-ethyl 1-ethyl-4-(tert-butyldimethylsilyloxy)-cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C

2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 76 h / 0 - 20 °C

3: potassium carbonate / methanol / 1 h / 20 °C

4: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

With 1H-imidazole; di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; potassium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;

Reference yield:

: 862728-41-4
trans-1-ethyl-4-hydroxy-cyclohexanecarboxylic acid ethyl ester

: 950772-73-3
trans-ethyl 1-ethyl-4-(tert-butyldimethylsilyloxy)-cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 76 h / 0 - 20 °C

2: potassium carbonate / methanol / 1 h / 20 °C

3: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

With 1H-imidazole; di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;