C₁₅H₂₁NO₅Si

Base Information

Chemical Name:C₁₅H₂₁NO₅Si
CAS No.:1265279-46-6
Molecular Formula:C₁₅H₂₁NO₅Si
Molecular Weight:323.421
Hs Code.:

C<sub>15</sub>H<sub>21</sub>NO<sub>5</sub>Si

Synonyms:C₁₅H₂₁NO₅Si

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Chemical Property of C₁₅H₂₁NO₅Si

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Technology Process of C₁₅H₂₁NO₅Si

There total 1 articles about C₁₅H₂₁NO₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1020070-44-3
2-(trimethylsilyl)-ethyl 3-amino-2,4-dihydroxybenzoate

: 79-10-7
acrylic acid

: 1265279-46-6
C₁₅H₂₁NO₅Si

Guidance literature:: With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In N,N-dimethyl-formamide; at 23 ℃; for 16h; Inert atmosphere;
DOI:10.1002/ejoc.201001281

Reference yield: 42.0%

: (2S,4aS,8S,8aR)-8-allyl-8-methyl-3-methylene-1,2,3,4,8,8a-hexahydro-7H-2,4a-ethanonaphthalen-7-one

: 1265279-46-6
C₁₅H₂₁NO₅Si

: 1265279-47-7
C₃₀H₃₉NO₆Si

Guidance literature:: With Hoveyda-Grubbs catalyst second generation; In benzene; at 70 ℃; for 1.17h; Inert atmosphere;
DOI:10.1002/ejoc.201001281

Reference yield:

: (2S,4aS,8S,8aR)-8-allyl-8-methyl-3-methylene-1,2,3,4,8,8a-hexahydro-7H-2,4a-ethanonaphthalen-7-one

: 1265279-46-6
C₁₅H₂₁NO₅Si

: 1265278-80-5
C₂₅H₂₇NO₆

Guidance literature:: Multi-step reaction with 2 steps

1: Hoveyda-Grubbs catalyst second generation / benzene / 1.17 h / 70 °C / Inert atmosphere

2: tris(dimethylamino)sulfonium trimethylsilyldifluoride; HATU / N,N-dimethyl-formamide / 1.33 h / 23 - 40 °C / Inert atmosphere

With Hoveyda-Grubbs catalyst second generation; tris(dimethylamino)sulfonium trimethylsilyldifluoride; HATU; In N,N-dimethyl-formamide; benzene;
DOI:10.1002/ejoc.201001281