3-azido-N-(4-chlorophenyl)-2-(dibenzo[b,d]furan-2-yl)-2-methylpropanamide

Base Information

Chemical Name:3-azido-N-(4-chlorophenyl)-2-(dibenzo[b,d]furan-2-yl)-2-methylpropanamide
CAS No.:1628741-43-4
Molecular Formula:C₂₃H₂₂N₄O₂
Molecular Weight:386.453
Hs Code.:

Synonyms:3-azido-N-(4-chlorophenyl)-2-(dibenzo[b,d]furan-2-yl)-2-methylpropanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-azido-N-(4-chlorophenyl)-2-(dibenzo[b,d]furan-2-yl)-2-methylpropanamide

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Technology Process of 3-azido-N-(4-chlorophenyl)-2-(dibenzo[b,d]furan-2-yl)-2-methylpropanamide

There total 3 articles about 3-azido-N-(4-chlorophenyl)-2-(dibenzo[b,d]furan-2-yl)-2-methylpropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1628741-18-3
C₂₃H₂₁NO₄S

: 1628741-43-4
3-azido-N-(4-chlorophenyl)-2-(dibenzo[b,d]furan-2-yl)-2-methylpropanamide

Guidance literature:: With 1-azido-1λ³-benzo[d][1,2]iodaoxol-3(1H)-one; In dichloromethane; at 60 ℃; for 14h; Inert atmosphere;
DOI:10.1002/anie.201311241

Reference yield:

: 51491-68-0
2-phenylacrylyl chloride

: 1628741-43-4
3-azido-N-(4-chlorophenyl)-2-(dibenzo[b,d]furan-2-yl)-2-methylpropanamide

Guidance literature:: Multi-step reaction with 2 steps

2: 1-azido-1λ³-benzo[d][1,2]iodaoxol-3(1H)-one / dichloromethane / 14 h / 60 °C / Inert atmosphere

With 1-azido-1λ³-benzo[d][1,2]iodaoxol-3(1H)-one; In dichloromethane;
DOI:10.1002/anie.201311241

Reference yield:

: 104-94-9
4-methoxy-aniline

: 1628741-43-4
3-azido-N-(4-chlorophenyl)-2-(dibenzo[b,d]furan-2-yl)-2-methylpropanamide

Guidance literature:: Multi-step reaction with 2 steps

2: 1-azido-1λ³-benzo[d][1,2]iodaoxol-3(1H)-one / dichloromethane / 14 h / 60 °C / Inert atmosphere

With 1-azido-1λ³-benzo[d][1,2]iodaoxol-3(1H)-one; In dichloromethane;
DOI:10.1002/anie.201311241