2-phenylacrylyl chloride

Base Information

Chemical Name:2-phenylacrylyl chloride
CAS No.:51491-68-0
Molecular Formula:C₉H₇ClO
Molecular Weight:166.607
Hs Code.:

Synonyms:2-phenylacrylyl chloride

Suppliers and Price of 2-phenylacrylyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2-phenylacrylyl chloride

Chemical Property:

Purity/Quality:: 99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-phenylacrylyl chloride

There total 13 articles about 2-phenylacrylyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 149423-39-2
tropoyl chloride

: 492-38-6
2-phenylacrylic acid

: 51491-68-0
2-phenylacrylyl chloride

Guidance literature:: bei der Destillation;

Reference yield:

: 492-38-6
2-phenylacrylic acid

: 51491-68-0
2-phenylacrylyl chloride

Guidance literature:: With thionyl chloride;

Reference yield:

: 103-82-2
phenylacetic acid

: 51491-68-0
2-phenylacrylyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid / 2 h / Reflux

2: potassium carbonate; tetra-(n-butyl)ammonium iodide / toluene / 12 h / 50 °C

3: sodium hydroxide / 2 h / Reflux

4: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 20 °C / Inert atmosphere

With oxalyl dichloride; sulfuric acid; tetra-(n-butyl)ammonium iodide; potassium carbonate; N,N-dimethyl-formamide; sodium hydroxide; In dichloromethane; toluene;
DOI:10.1002/anie.201700195