C₁₂H₁₈O₂

Base Information

Chemical Name:C₁₂H₁₈O₂
CAS No.:1390644-46-8
Molecular Formula:C₁₂H₁₈O₂
Molecular Weight:194.274
Hs Code.:

C<sub>12</sub>H<sub>18</sub>O<sub>2</sub>

Synonyms:C₁₂H₁₈O₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₂H₁₈O₂

Chemical Property:

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Technology Process of C₁₂H₁₈O₂

There total 1 articles about C₁₂H₁₈O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 2100-17-6
4-pentenal

: 54307-74-3,15466-88-3
(R)-5-methyl-cyclohex-2-enone

: 1390644-46-8
C₁₂H₁₈O₂

Guidance literature:: With tributylphosphine; 1,1'-binaphthyl-8,8'-diol; In tetrahydrofuran; at 20 ℃; for 96h; Inert atmosphere;
DOI:10.1021/ja305261h

Reference yield: 100.0%

: 1390644-46-8
C₁₂H₁₈O₂

: 1390644-48-0
C₁₂H₁₆O₂

Guidance literature:: With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; at 0 - 20 ℃; for 2h;
DOI:10.1021/ja305261h

Reference yield:

: 1390644-46-8
C₁₂H₁₈O₂

: 1390644-55-9
C₂₄H₃₃NO₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 2 h / 0 - 20 °C

2.1: lithium perchlorate / dichloromethane / 1 h / 20 °C

3.1: triethylamine / N,N-dimethyl-formamide / 20 °C

4.1: sodium triacetoxy borohydride; acetic acid / 1,1-dichloroethane / 12 h / -30 - 20 °C

5.1: H₄O₆Os^(2-)*K⁽¹⁺⁾; 4-methylmorpholine N-oxide / water; acetone

5.2: 3 h / 20 °C

With sodium triacetoxy borohydride; H₄O₆Os^(2-)*K⁽¹⁺⁾; lithium perchlorate; sodium hydrogencarbonate; Dess-Martin periodane; acetic acid; 4-methylmorpholine N-oxide; triethylamine; In 1,1-dichloroethane; dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1021/ja305261h