Methyl 4-(14-(tert-butyldimethylsilyloxy)tetradec-1-ynyl)-3,5-dimethoxybenzoate

Base Information

Chemical Name:Methyl 4-(14-(tert-butyldimethylsilyloxy)tetradec-1-ynyl)-3,5-dimethoxybenzoate
CAS No.:947735-93-5
Molecular Formula:C₃₀H₅₀O₅Si
Molecular Weight:518.809
Hs Code.:

Synonyms:Methyl 4-(14-(tert-butyldimethylsilyloxy)tetradec-1-ynyl)-3,5-dimethoxybenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl 4-(14-(tert-butyldimethylsilyloxy)tetradec-1-ynyl)-3,5-dimethoxybenzoate

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Technology Process of Methyl 4-(14-(tert-butyldimethylsilyloxy)tetradec-1-ynyl)-3,5-dimethoxybenzoate

There total 1 articles about Methyl 4-(14-(tert-butyldimethylsilyloxy)tetradec-1-ynyl)-3,5-dimethoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: tert-butyl(tetradec-13-ynyloxy)dimethylsilane

: 65566-16-7
methyl 4-iodo-3,5-dimethoxybenzoate

: 947735-93-5
Methyl 4-(14-(tert-butyldimethylsilyloxy)tetradec-1-ynyl)-3,5-dimethoxybenzoate

Guidance literature:: With triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In triethylamine; at 20 ℃; Reflux;

Reference yield: 95.0%

: 947735-93-5
Methyl 4-(14-(tert-butyldimethylsilyloxy)tetradec-1-ynyl)-3,5-dimethoxybenzoate

: 947735-94-6
Methyl 4-(14-(tert-butyldimethylsilyloxy)tetradecyl)-3,5-dimethoxybenzoate

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In ethanol; at 20 ℃; for 24h;

Reference yield:

: 947735-93-5
Methyl 4-(14-(tert-butyldimethylsilyloxy)tetradec-1-ynyl)-3,5-dimethoxybenzoate

: 947735-95-7
(4-(14-(tert-butyldimethylsilyloxy)tetradecyl)-3,5-dimethoxyphenyl)methanol

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / ethanol / 24 h / 20 °C

2: LiAlH₄ / tetrahydrofuran / 2 h / 0 - 20 °C

With lithium aluminium tetrahydride; hydrogen; palladium on activated charcoal; In tetrahydrofuran; ethanol;
DOI:10.1016/j.bmcl.2007.05.037