C₁₆H₉Br₂F₃

Base Information

Chemical Name:C₁₆H₉Br₂F₃
CAS No.:947546-76-1
Molecular Formula:C₁₆H₉Br₂F₃
Molecular Weight:418.051
Hs Code.:

C<sub>16</sub>H<sub>9</sub>Br<sub>2</sub>F<sub>3</sub>

Synonyms:C₁₆H₉Br₂F₃

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Chemical Property of C₁₆H₉Br₂F₃

Chemical Property:

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Technology Process of C₁₆H₉Br₂F₃

There total 3 articles about C₁₆H₉Br₂F₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 935223-82-8
2-bromo-4-methyl-1-[2-(trimethylsilyl)ethynyl]benzene

: 947546-76-1
C₁₆H₉Br₂F₃

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / K₂CO₃ / CH₂Cl₂; methanol / 12 h / 20 °C

2: 85 percent / triethylamine / Pd(PPh₃)4; CuI / 6 h / 60 °C

With potassium carbonate; triethylamine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; dichloromethane;
DOI:10.1002/anie.200700022

Reference yield:

: 71838-16-9
3-bromo-4-iodotoluene

: 947546-76-1
C₁₆H₉Br₂F₃

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / triethylamine / Pd(PPh₃)4; CuI / 3 h / 60 °C

2: 90 percent / K₂CO₃ / CH₂Cl₂; methanol / 12 h / 20 °C

3: 85 percent / triethylamine / Pd(PPh₃)4; CuI / 6 h / 60 °C

With potassium carbonate; triethylamine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; dichloromethane;
DOI:10.1002/anie.200700022

Reference yield:

2-bromo-p-toluidine: 583-68-6
2-bromo-p-toluidine

: 947546-76-1
C₁₆H₉Br₂F₃

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / NaNO₂; KI; H₂SO₄ / H₂O / 4 h / 0 - 20 °C

2: 91 percent / triethylamine / Pd(PPh₃)4; CuI / 3 h / 60 °C

3: 90 percent / K₂CO₃ / CH₂Cl₂; methanol / 12 h / 20 °C

4: 85 percent / triethylamine / Pd(PPh₃)4; CuI / 6 h / 60 °C

With sulfuric acid; potassium carbonate; triethylamine; potassium iodide; sodium nitrite; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; dichloromethane; water;
DOI:10.1002/anie.200700022