1-bromocyclopropyl benzyl sulfide

Base Information

• Chemical Name: 1-bromocyclopropyl benzyl sulfide
• CAS No.: 78709-02-1
• Molecular Formula: C₁₀H₁₁BrS
• Molecular Weight: 243.167
• Mol file: 78709-02-1.mol

Synonyms:1-bromocyclopropyl benzyl sulfide

Chemical Property of 1-bromocyclopropyl benzyl sulfide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 1-bromocyclopropyl benzyl sulfide

There total 2 articles about 1-bromocyclopropyl benzyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1-(benzylthio)cyclopropanol (79306-16-4) → 1-bromocyclopropyl benzyl sulfide (78709-02-1)

Guidance literature:

With hydrogen bromide; In dichloromethane; at 0 ℃; for 1h;

Reference yield:

phenylmethanethiol (100-53-8) → 1-bromocyclopropyl benzyl sulfide (78709-02-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 60 percent / CH₂Cl₂ / 16 h / -30 °C

2: 95 percent / hydrogen bromide / CH₂Cl₂ / 1 h / 0 °C

With hydrogen bromide; In dichloromethane;

Reference yield: 100.0%

2,2,2-trifluoroethanol (75-89-8) + 1-bromocyclopropyl benzyl sulfide (78709-02-1) → [1-(2,2,2-Trifluoro-ethoxy)-cyclopropylsulfanylmethyl]-benzene

Guidance literature:

at 0 ℃;

upstream raw materials:

1-(benzylthio)cyclopropanol

phenylmethanethiol

Downstream raw materials:

di-tert-butyl disulfide

Refernces