Benzoic acid (1R,2R,6R)-2-azido-6-hydroxy-4-methoxycarbonyl-cyclohex-3-enyl ester

Base Information

• Chemical Name: Benzoic acid (1R,2R,6R)-2-azido-6-hydroxy-4-methoxycarbonyl-cyclohex-3-enyl ester
• CAS No.: 179927-04-9
• Molecular Formula: C₁₅H₁₅N₃O₅
• Molecular Weight: 317.301

Synonyms:Benzoic acid (1R,2R,6R)-2-azido-6-hydroxy-4-methoxycarbonyl-cyclohex-3-enyl ester

Chemical Property of Benzoic acid (1R,2R,6R)-2-azido-6-hydroxy-4-methoxycarbonyl-cyclohex-3-enyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzoic acid (1R,2R,6R)-2-azido-6-hydroxy-4-methoxycarbonyl-cyclohex-3-enyl ester

There total 2 articles about Benzoic acid (1R,2R,6R)-2-azido-6-hydroxy-4-methoxycarbonyl-cyclohex-3-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

Benzoic acid (1S,2S,6R)-2-bromo-6-hydroxy-4-methoxycarbonyl-cyclohex-3-enyl ester (179738-33-1) → Benzoic acid (1R,2R,6R)-2-azido-6-hydroxy-4-methoxycarbonyl-cyclohex-3-enyl ester (179927-04-9) + Benzoic acid (1R,5R,6R)-5-azido-6-hydroxy-3-methoxycarbonyl-cyclohex-3-enyl ester (179927-08-3) + (1R,5S,6R)-5-azido-6-hydroxy-3-(methoxycarbonyl)-3-cyclohexen-1-yl benzoate (180061-38-5)

Guidance literature:

With sodium azide; In methanol; at 40 ℃;

DOI:10.1016/0040-4020(96)00398-5

Reference yield: 8.0%

Benzoic acid (1S,2S,6R)-2-bromo-6-hydroxy-4-methoxycarbonyl-cyclohex-3-enyl ester (179738-33-1) → Benzoic acid (1R,2R,6R)-2-azido-6-hydroxy-4-methoxycarbonyl-cyclohex-3-enyl ester (179927-04-9) + Benzoic acid (1R,5R,6R)-5-azido-6-hydroxy-3-methoxycarbonyl-cyclohex-3-enyl ester (179927-08-3) + Benzoic acid (1R,2S,6R)-2-azido-6-hydroxy-4-methoxycarbonyl-cyclohex-3-enyl ester

Guidance literature:

With sodium azide; In methanol; at 40 ℃;

DOI:10.1016/0960-894X(96)00011-X

Reference yield: 84.0%

Benzoic acid (1R,2R,6R)-2-azido-6-hydroxy-4-methoxycarbonyl-cyclohex-3-enyl ester (179927-04-9) → methyl (3R,4S,5R)-3-azido-4,5-dihydroxy-cyclohex-1-en-1-carboxylate (179927-12-9)

Guidance literature:

With sodium methylate; In methanol; at 0 ℃; for 3h;

DOI:10.1016/0040-4020(96)00398-5

upstream raw materials:

Benzoic acid (1S,2S,6R)-2-bromo-6-hydroxy-4-methoxycarbonyl-cyclohex-3-enyl ester

Downstream raw materials:

methyl (3R,4S,5R)-3-azido-4,5-dihydroxy-cyclohex-1-en-1-carboxylate

(3R,4R,5R)-3-Amino-4,5-dihydroxy-cyclohex-1-enecarboxylic acid methyl ester

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 179927-04-9 Benzoic acid (1R,2R,6R)-2-azido-6-hydroxy-4-methoxycarbonyl-cyclohex-3-enyl ester

Send

Send

Metric Ton KG G Pound L ML

Send

Send