4-cyclohexyl-1,4-dihydro-2-methoxy-6-methyl-5-pyrimidinecarboxylic acid ethyl ester

Base Information

Chemical Name:4-cyclohexyl-1,4-dihydro-2-methoxy-6-methyl-5-pyrimidinecarboxylic acid ethyl ester
CAS No.:123486-05-5
Molecular Formula:C₁₅H₂₄N₂O₃
Molecular Weight:280.367
Hs Code.:

Synonyms:4-cyclohexyl-1,4-dihydro-2-methoxy-6-methyl-5-pyrimidinecarboxylic acid ethyl ester

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Chemical Property of 4-cyclohexyl-1,4-dihydro-2-methoxy-6-methyl-5-pyrimidinecarboxylic acid ethyl ester

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Technology Process of 4-cyclohexyl-1,4-dihydro-2-methoxy-6-methyl-5-pyrimidinecarboxylic acid ethyl ester

There total 1 articles about 4-cyclohexyl-1,4-dihydro-2-methoxy-6-methyl-5-pyrimidinecarboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 29427-58-5,24285-39-0
O-methylisourea hemisulfate

: 89082-76-8
2-(cyclohexanylmethylene)-3-oxobutanoic acid ethyl ester

: 123486-05-5
4-cyclohexyl-1,4-dihydro-2-methoxy-6-methyl-5-pyrimidinecarboxylic acid ethyl ester

Guidance literature:: With sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 70 ℃; for 24h;
DOI:10.1021/jo00286a020

Reference yield:

: 123486-05-5
4-cyclohexyl-1,4-dihydro-2-methoxy-6-methyl-5-pyrimidinecarboxylic acid ethyl ester

: 123486-01-1
6-cyclohexyl-3,6-dihydro-4-methyl-2-oxo-1,5(2H)-pyrimidinedicarboxylic acid bis(ethyl ester)

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / CH₂Cl₂ / 0.5 h / Ambient temperature

2: 2 N aq. HCl / methanol / 0.5 h / Ambient temperature

With pyridine; hydrogenchloride; In methanol; dichloromethane;
DOI:10.1021/jo00286a020