C₂₅H₂₂ClNO₃

Base Information

Chemical Name:C₂₅H₂₂ClNO₃
CAS No.:1359022-68-6
Molecular Formula:C₂₅H₂₂ClNO₃
Molecular Weight:419.908
Hs Code.:

C<sub>25</sub>H<sub>22</sub>ClNO<sub>3</sub>

Synonyms:C₂₅H₂₂ClNO₃

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Chemical Property of C₂₅H₂₂ClNO₃

Chemical Property:

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Technology Process of C₂₅H₂₂ClNO₃

There total 11 articles about C₂₅H₂₂ClNO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50868-73-0
2-methoxy-6-methylbenzeneamine

: 1359022-68-6
C₂₅H₂₂ClNO₃

Guidance literature:: Multi-step reaction with 10 steps

1.1: bromine; acetic acid / methanol / 2 h / 20 °C / Cooling with ice

2.1: hydrogenchloride; sodium nitrite / water / 0.5 h / 0 °C

2.2: 4 h / 0 - 50 °C

3.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / -78 - 20 °C

3.2: 1 h / 20 °C

4.1: sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 0.5 h / 20 °C

4.2: pH 1

5.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

6.1: triethylamine / dmap / 1 h / 20 °C

7.1: N-chloro-succinimide / acetonitrile / 45 h / 60 °C

8.1: boron tribromide / dichloromethane / 0.75 h / -78 - 0 °C

8.2: 0.17 h / 20 °C

9.1: potassium carbonate / acetone / 20 °C

10.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -100 °C / Inert atmosphere

10.2: 2 h / -78 °C

With hydrogenchloride; sodium chlorite; sodium dihydrogenphosphate; N-chloro-succinimide; n-butyllithium; 2-methyl-but-2-ene; oxalyl dichloride; bromine; boron tribromide; diisobutylaluminium hydride; potassium carbonate; acetic acid; triethylamine; sodium nitrite; dmap; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; hexane; dichloromethane; water; acetone; toluene; acetonitrile; tert-butyl alcohol;

Reference yield:

: 877149-05-8
4-bromo-2-methoxy-6-methyl-benzonitrile

: 1359022-68-6
C₂₅H₂₂ClNO₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / -78 - 20 °C

1.2: 1 h / 20 °C

2.1: sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 0.5 h / 20 °C

2.2: pH 1

3.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

4.1: triethylamine / dmap / 1 h / 20 °C

5.1: N-chloro-succinimide / acetonitrile / 45 h / 60 °C

6.1: boron tribromide / dichloromethane / 0.75 h / -78 - 0 °C

6.2: 0.17 h / 20 °C

7.1: potassium carbonate / acetone / 20 °C

8.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -100 °C / Inert atmosphere

8.2: 2 h / -78 °C

With sodium chlorite; sodium dihydrogenphosphate; N-chloro-succinimide; n-butyllithium; 2-methyl-but-2-ene; oxalyl dichloride; boron tribromide; diisobutylaluminium hydride; potassium carbonate; triethylamine; dmap; N,N-dimethyl-formamide; In tetrahydrofuran; hexane; dichloromethane; water; acetone; toluene; acetonitrile; tert-butyl alcohol;

Reference yield:

: 877149-08-1
4-bromo-2-methoxy-6-methyl-benzoic acid

: 1359022-68-6
C₂₅H₂₂ClNO₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

2.1: triethylamine / dmap / 1 h / 20 °C

3.1: N-chloro-succinimide / acetonitrile / 45 h / 60 °C

4.1: boron tribromide / dichloromethane / 0.75 h / -78 - 0 °C

4.2: 0.17 h / 20 °C

5.1: potassium carbonate / acetone / 20 °C

6.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -100 °C / Inert atmosphere

6.2: 2 h / -78 °C

With N-chloro-succinimide; n-butyllithium; oxalyl dichloride; boron tribromide; potassium carbonate; triethylamine; dmap; N,N-dimethyl-formamide; In tetrahydrofuran; hexane; dichloromethane; acetone; acetonitrile;