3-methoxy-2-{[(4-methylphenyl)sulfonyl]oxy}benzoic acid

Base Information

Chemical Name:3-methoxy-2-{[(4-methylphenyl)sulfonyl]oxy}benzoic acid
CAS No.:93945-52-9
Molecular Formula:C15H14 O6 S
Molecular Weight:322.3331
Hs Code.:

Synonyms:m-Anisicacid, 2-hydroxy-, p-toluenesulfonate (7CI); NSC 283851

Suppliers and Price of 3-methoxy-2-{[(4-methylphenyl)sulfonyl]oxy}benzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 3-methoxy-2-{[(4-methylphenyl)sulfonyl]oxy}benzoic acid

Chemical Property:

Vapor Pressure:7.85E-12mmHg at 25°C
Boiling Point:524.6°Cat760mmHg
Flash Point:271°C
Density:1.366g/cm³

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-methoxy-2-{[(4-methylphenyl)sulfonyl]oxy}benzoic acid

There total 3 articles about 3-methoxy-2-{[(4-methylphenyl)sulfonyl]oxy}benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 7740-04-7
3-methoxy-2-<(p-tolylsulfonyl)oxy>benzaldehyde

: 93945-52-9
2-p-Toluolsulfonyloxy-3-methoxy-benzoesaeure

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; dihydrogen peroxide; sodium sulfite; In water; acetonitrile; Inert atmosphere;
DOI:10.3987/COM-17-S(T)6

Reference yield:

: 148-53-8
3-methoxy-2-hydroxybenzaldehyde

: 93945-52-9
2-p-Toluolsulfonyloxy-3-methoxy-benzoesaeure

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / dichloromethane; water / Inert atmosphere

2: sodium chlorite; sodium dihydrogenphosphate; dihydrogen peroxide; sodium sulfite / water; acetonitrile / Inert atmosphere

With sodium chlorite; sodium dihydrogenphosphate; dihydrogen peroxide; sodium hydroxide; sodium sulfite; In dichloromethane; water; acetonitrile;
DOI:10.3987/COM-17-S(T)6

Reference yield:

: 93945-52-9
2-p-Toluolsulfonyloxy-3-methoxy-benzoesaeure

Guidance literature:: 2-p-Toluolsulfonyloxy-3-methoxy-benzaldehyd, KMnO4, wss. MgSO4, 80grad, neben 2-<4-Carboxy-benzolsulfonyloxy>-3-methoxy-benzoesaeure;
DOI:10.1002/ardp.19642970405