5-chloro-4-(3-chloro-4-(trifluoromethyl)phenoxy)-2-fluoro-N-(methylsulfonyl)benzamide

Base Information

Chemical Name:5-chloro-4-(3-chloro-4-(trifluoromethyl)phenoxy)-2-fluoro-N-(methylsulfonyl)benzamide
CAS No.:1354955-52-4
Molecular Formula:C₁₅H₉Cl₂F₄NO₄S
Molecular Weight:446.206
Hs Code.:

Synonyms:5-chloro-4-(3-chloro-4-(trifluoromethyl)phenoxy)-2-fluoro-N-(methylsulfonyl)benzamide

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Chemical Property of 5-chloro-4-(3-chloro-4-(trifluoromethyl)phenoxy)-2-fluoro-N-(methylsulfonyl)benzamide

Chemical Property:

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Technology Process of 5-chloro-4-(3-chloro-4-(trifluoromethyl)phenoxy)-2-fluoro-N-(methylsulfonyl)benzamide

There total 4 articles about 5-chloro-4-(3-chloro-4-(trifluoromethyl)phenoxy)-2-fluoro-N-(methylsulfonyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 4.9%

: 1354960-67-0
5-chloro-2,4-difluoro-N-(methylsulfonyl)benzamide

: 37900-81-5
2-chloro-4-hydroxybenzotrifluoride

: 1354955-52-4
5-chloro-4-(3-chloro-4-(trifluoromethyl)phenoxy)-2-fluoro-N-(methylsulfonyl)benzamide

Guidance literature:: With potassium carbonate; In dimethyl sulfoxide; at 90 ℃; for 18h; Inert atmosphere;

Reference yield:

: 94444-58-3
2-chloro-4-fluoro-1-(trifluoromethyl)benzene

: 1354955-52-4
5-chloro-4-(3-chloro-4-(trifluoromethyl)phenoxy)-2-fluoro-N-(methylsulfonyl)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / tetrahydrofuran; mineral oil / 18 h / 20 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / 1,4-dioxane; tetrahydrofuran / 18 h / 20 °C / Inert atmosphere

3: potassium carbonate / dimethyl sulfoxide / 18 h / 90 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; sodium hydride; potassium carbonate; In tetrahydrofuran; 1,4-dioxane; dimethyl sulfoxide; mineral oil;

Reference yield:

: 1354960-72-7
(2-(3-chloro-4-(trifluoromethyl)phenoxy)ethyl)trimethylsilane

: 1354955-52-4
5-chloro-4-(3-chloro-4-(trifluoromethyl)phenoxy)-2-fluoro-N-(methylsulfonyl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / 1,4-dioxane; tetrahydrofuran / 18 h / 20 °C / Inert atmosphere

2: potassium carbonate / dimethyl sulfoxide / 18 h / 90 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; potassium carbonate; In tetrahydrofuran; 1,4-dioxane; dimethyl sulfoxide;