methyl 3-O-(4-O-benzoyl-3-O-benzyl-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-α-D-arabino-hexopyranoside

Base Information

Chemical Name:methyl 3-O-(4-O-benzoyl-3-O-benzyl-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-α-D-arabino-hexopyranoside
CAS No.:121330-40-3
Molecular Formula:C₂₇H₃₄O₈
Molecular Weight:486.562
Hs Code.:

Synonyms:methyl 3-O-(4-O-benzoyl-3-O-benzyl-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-α-D-arabino-hexopyranoside

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Chemical Property of methyl 3-O-(4-O-benzoyl-3-O-benzyl-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-α-D-arabino-hexopyranoside

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Technology Process of methyl 3-O-(4-O-benzoyl-3-O-benzyl-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-α-D-arabino-hexopyranoside

There total 6 articles about methyl 3-O-(4-O-benzoyl-3-O-benzyl-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-α-D-arabino-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 121330-37-8
Methyl 3-O-(4-O-Benzoyl-3-O-benzyl-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-4-O-(p-tolylsulfonyl)-α-D-arabino-hexopyranoside

: 121330-40-3
methyl 3-O-(4-O-benzoyl-3-O-benzyl-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-α-D-arabino-hexopyranoside

Guidance literature:: With triethylamine; In methanol; for 1h; Irradiation;
DOI:10.1021/jo00276a015

Reference yield:

: 121330-33-4
Methyl 3-O-Benzyl-2,6-dideoxy-4-O-(p-tolylsulfonyl)-α-D-arabino-hexopyranoside

: 121330-40-3
methyl 3-O-(4-O-benzoyl-3-O-benzyl-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-α-D-arabino-hexopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / H₂ / 5percent Pd/C / methanol / 24 h / 760 Torr

2: 77 percent / silver silicate / toluene / 12 h

3: 80 percent / 0.02 M triethylamine / methanol / 1 h / Irradiation

With silver silicate; hydrogen; triethylamine; palladium on activated charcoal; In methanol; toluene;
DOI:10.1021/jo00276a015

Reference yield:

: 90762-83-7
Methyl 3-O-benzyl-2,6-dideoxy-α-D-arabino-hexopyranoside

: 121330-40-3
methyl 3-O-(4-O-benzoyl-3-O-benzyl-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-α-D-arabino-hexopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / pyridine / 13 h / 55 - 60 °C

2: 90 percent / H₂ / 5percent Pd/C / methanol / 24 h / 760 Torr

3: 77 percent / silver silicate / toluene / 12 h

4: 80 percent / 0.02 M triethylamine / methanol / 1 h / Irradiation

With pyridine; silver silicate; hydrogen; triethylamine; palladium on activated charcoal; In methanol; toluene;
DOI:10.1021/jo00276a015