10-(6-hydroxy-hexyl)-6-nitro-3-phenyl-10H-pyrimido[4,5-b]quinoline-2,4-dione

Base Information

• Chemical Name: 10-(6-hydroxy-hexyl)-6-nitro-3-phenyl-10H-pyrimido[4,5-b]quinoline-2,4-dione
• CAS No.: 302897-04-7
• Molecular Formula: C₂₃H₂₂N₄O₅
• Molecular Weight: 434.451

Synonyms:10-(6-hydroxy-hexyl)-6-nitro-3-phenyl-10H-pyrimido[4,5-b]quinoline-2,4-dione

Chemical Property of 10-(6-hydroxy-hexyl)-6-nitro-3-phenyl-10H-pyrimido[4,5-b]quinoline-2,4-dione

Chemical Property:

Purity/Quality:

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Technology Process of 10-(6-hydroxy-hexyl)-6-nitro-3-phenyl-10H-pyrimido[4,5-b]quinoline-2,4-dione

There total 5 articles about 10-(6-hydroxy-hexyl)-6-nitro-3-phenyl-10H-pyrimido[4,5-b]quinoline-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

2-fluoro-6-nitrobenzaldehyde (1644-82-2) + 6-(6-hydroxyhexyl)amino-3-phenyluracil (302897-03-6) → 10-(6-hydroxy-hexyl)-6-nitro-3-phenyl-10H-pyrimido[4,5-b]quinoline-2,4-dione (302897-04-7)

Guidance literature:

In N,N-dimethyl-formamide; at 120 ℃; for 3h;

DOI:10.1016/S0968-0896(00)00124-3

Reference yield:

10-[6-O-(methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosylonate)hexyl]-6-nitro-3-phenyl-5-deazaflavin (302897-08-1) → 10-(6-hydroxy-hexyl)-6-nitro-3-phenyl-10H-pyrimido[4,5-b]quinoline-2,4-dione (302897-04-7)

Guidance literature:

With acetic acid; In water; at 100 ℃; for 6h; Product distribution;

DOI:10.1016/S0968-0896(00)00124-3

Reference yield:

10-[6-O-(methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-β-D-galacto-non-2-ulopyranosylonate)hexyl]-6-nitro-3-phenyl-5-deazaflavin (302897-00-3) → 10-(6-hydroxy-hexyl)-6-nitro-3-phenyl-10H-pyrimido[4,5-b]quinoline-2,4-dione (302897-04-7)

Guidance literature:

With acetic acid; In water; at 100 ℃; for 6h; Product distribution;

DOI:10.1016/S0968-0896(00)00124-3

upstream raw materials:

2-fluoro-6-nitrobenzaldehyde

6-(6-hydroxyhexyl)amino-3-phenyluracil

10-[6-O-(methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-β-D-galacto-non-2-ulopyranosylonate)hexyl]-6-nitro-3-phenyl-5-deazaflavin

10-[6-O-(methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosylonate)hexyl]-6-nitro-3-phenyl-5-deazaflavin

Downstream raw materials:

10-[6-O-(methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-β-D-galacto-non-2-ulopyranosylonate)hexyl]-6-nitro-3-phenyl-5-deazaflavin

10-[6-O-(methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosylonate)hexyl]-6-nitro-3-phenyl-5-deazaflavin

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