C₂₀H₃₁N₃O₂

Base Information

Chemical Name:C₂₀H₃₁N₃O₂
CAS No.:1063410-18-3
Molecular Formula:C₂₀H₃₁N₃O₂
Molecular Weight:345.485
Hs Code.:

C<sub>20</sub>H<sub>31</sub>N<sub>3</sub>O<sub>2</sub>

Synonyms:C₂₀H₃₁N₃O₂

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Chemical Property of C₂₀H₃₁N₃O₂

Chemical Property:

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Technology Process of C₂₀H₃₁N₃O₂

There total 8 articles about C₂₀H₃₁N₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₆H₄₇N₃O₂Si₂

: 1063410-18-3
C₂₀H₃₁N₃O₂

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; hexane; at 20 ℃; Sealed tube; Inert atmosphere;
DOI:10.1016/j.ejmech.2012.07.006

Reference yield:

: 4746-97-8
cyclohexanedione monoethylene ketal

: 1063410-18-3
C₂₀H₃₁N₃O₂

Guidance literature:: Multi-step reaction with 7 steps

1: sodium cyanoborohydride; acetic acid / 1,2-dichloro-ethane / 20 °C / Inert atmosphere

2: N-Bromosuccinimide / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

3: hydrogenchloride / water; acetone / 16 h / 20 °C / Inert atmosphere

4: sodium cyanoborohydride; acetic acid / methanol / 0 - 20 °C / Inert atmosphere

5: triethylamine / 1,4-dioxane / 20 °C / Inert atmosphere

6: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; lithium hexamethyldisilazane / tetrahydrofuran; hexane / 20 - 100 °C / Sealed tube; Inert atmosphere

7: tetrabutyl ammonium fluoride / tetrahydrofuran; hexane / 20 °C / Sealed tube; Inert atmosphere

With hydrogenchloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N-Bromosuccinimide; tri-tert-butyl phosphine; tetrabutyl ammonium fluoride; sodium cyanoborohydride; acetic acid; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; 1,4-dioxane; methanol; hexane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone; 6: |Buchwald-Hartwig Coupling;
DOI:10.1016/j.ejmech.2012.07.006

Reference yield:

: 1063410-05-8
1-(1,4-dioxaspiro[4.5]decan-8-yl)indoline

: 1063410-18-3
C₂₀H₃₁N₃O₂

Guidance literature:: Multi-step reaction with 6 steps

1: N-Bromosuccinimide / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

2: hydrogenchloride / water; acetone / 16 h / 20 °C / Inert atmosphere

3: sodium cyanoborohydride; acetic acid / methanol / 0 - 20 °C / Inert atmosphere

4: triethylamine / 1,4-dioxane / 20 °C / Inert atmosphere

5: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; lithium hexamethyldisilazane / tetrahydrofuran; hexane / 20 - 100 °C / Sealed tube; Inert atmosphere

6: tetrabutyl ammonium fluoride / tetrahydrofuran; hexane / 20 °C / Sealed tube; Inert atmosphere

With hydrogenchloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N-Bromosuccinimide; tri-tert-butyl phosphine; tetrabutyl ammonium fluoride; sodium cyanoborohydride; acetic acid; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; 1,4-dioxane; methanol; hexane; water; N,N-dimethyl-formamide; acetone; 5: |Buchwald-Hartwig Coupling;
DOI:10.1016/j.ejmech.2012.07.006