4,9-Dihydro-4,4,9,9-tetrakis(4-hexylphenyl)-s-indaceno[1,2-b:5,6-b']dithiophene

Base Information

Chemical Name:4,9-Dihydro-4,4,9,9-tetrakis(4-hexylphenyl)-s-indaceno[1,2-b:5,6-b']dithiophene
CAS No.:1049034-67-4
Molecular Formula:C₆₄H₇₄S₂
Molecular Weight:907.424
Hs Code.:
Mol file:1049034-67-4.mol

Synonyms:4,4,9,9-tetrakis(4-hexylphenyl)-4,9-dihydro-s-indaceno[1,2-b:5,6-b’]dithiophene

Suppliers and Price of 4,9-Dihydro-4,4,9,9-tetrakis(4-hexylphenyl)-s-indaceno[1,2-b:5,6-b']dithiophene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 11 raw suppliers

Chemical Property of 4,9-Dihydro-4,4,9,9-tetrakis(4-hexylphenyl)-s-indaceno[1,2-b:5,6-b']dithiophene

Chemical Property:

Purity/Quality:: 99%, ^*data from raw suppliers

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Technology Process of 4,9-Dihydro-4,4,9,9-tetrakis(4-hexylphenyl)-s-indaceno[1,2-b:5,6-b']dithiophene

There total 8 articles about 4,9-Dihydro-4,4,9,9-tetrakis(4-hexylphenyl)-s-indaceno[1,2-b:5,6-b']dithiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1049034-65-2
C₆₄H₇₈O₂S₂

: 1049034-67-4
4,4,9,9-tetrakis(4-hexylphenyl)-4,9-dihydro-s-indaceno[1,2-b:5,6-b’]dithiophene

Guidance literature:: With sulfuric acid; acetic acid; In n-heptane; at 70 ℃; for 3h;

Reference yield: 65.0%

: 915224-39-4
diethyl 1,4-bis(thiophen-2-yl)-2,5-benzenedicarboxylate

: (4-n-hexylphenyl)magnesium bromide

: 1049034-67-4
4,4,9,9-tetrakis(4-hexylphenyl)-4,9-dihydro-s-indaceno[1,2-b:5,6-b’]dithiophene

Guidance literature:: diethyl 1,4-bis(thiophen-2-yl)-2,5-benzenedicarboxylate; (4-n-hexylphenyl)magnesium bromide;

With hydrogenchloride; acetic acid;
DOI:10.1039/c0cc01087a

Reference yield: 45.0%

: 915224-39-4
diethyl 1,4-bis(thiophen-2-yl)-2,5-benzenedicarboxylate

: 23703-22-2
1-bromo-4-n-hexylbenzene

: 1049034-67-4
4,4,9,9-tetrakis(4-hexylphenyl)-4,9-dihydro-s-indaceno[1,2-b:5,6-b’]dithiophene

Guidance literature:: 1-bromo-4-n-hexylbenzene; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;

diethyl 1,4-bis(thiophen-2-yl)-2,5-benzenedicarboxylate; In tetrahydrofuran; at -78 ℃; for 1h; Further stages; Inert atmosphere;
DOI:10.1016/j.dyepig.2020.109116