N-[5-(5-bromo-2-methoxybenzenesulfonyl)-2-methoxyphenyl]-2,2,2-trifluoroacetamide

Base Information

Chemical Name:N-[5-(5-bromo-2-methoxybenzenesulfonyl)-2-methoxyphenyl]-2,2,2-trifluoroacetamide
CAS No.:1335406-99-9
Molecular Formula:C₁₆H₁₃BrF₃NO₅S
Molecular Weight:468.248
Hs Code.:

Synonyms:N-[5-(5-bromo-2-methoxybenzenesulfonyl)-2-methoxyphenyl]-2,2,2-trifluoroacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[5-(5-bromo-2-methoxybenzenesulfonyl)-2-methoxyphenyl]-2,2,2-trifluoroacetamide

Chemical Property:

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Technology Process of N-[5-(5-bromo-2-methoxybenzenesulfonyl)-2-methoxyphenyl]-2,2,2-trifluoroacetamide

There total 3 articles about N-[5-(5-bromo-2-methoxybenzenesulfonyl)-2-methoxyphenyl]-2,2,2-trifluoroacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104-92-7
1-bromo-4-methoxy-benzene

: 1184086-20-1
4-methoxy-3-(2,2,2-trifluoroacetamido)benzenesulfonyl chloride

: 1335406-99-9
N-[5-(5-bromo-2-methoxybenzenesulfonyl)-2-methoxyphenyl]-2,2,2-trifluoroacetamide

Guidance literature:: With aluminum (III) chloride; In 1,2-dichloro-ethane; for 20h; Inert atmosphere; Reflux;

Reference yield:

: 90-04-0
2-methoxy-phenylamine

: 1335406-99-9
N-[5-(5-bromo-2-methoxybenzenesulfonyl)-2-methoxyphenyl]-2,2,2-trifluoroacetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine / dichloromethane / 0.5 h / 0 °C

1.2: 1.25 h / 0 - 30 °C

2.1: chlorosulfonic acid / dichloromethane / 0 - 30 °C

3.1: aluminum (III) chloride / 1,2-dichloro-ethane / 20 h / Inert atmosphere; Reflux

With pyridine; chlorosulfonic acid; aluminum (III) chloride; In dichloromethane; 1,2-dichloro-ethane;

Reference yield:

: 14815-12-4
N-(2-methoxyphenyl)-2,2,2-trifluoro-acetamide

: 1335406-99-9
N-[5-(5-bromo-2-methoxybenzenesulfonyl)-2-methoxyphenyl]-2,2,2-trifluoroacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: chlorosulfonic acid / dichloromethane / 0 - 30 °C

2: aluminum (III) chloride / 1,2-dichloro-ethane / 20 h / Inert atmosphere; Reflux

With chlorosulfonic acid; aluminum (III) chloride; In dichloromethane; 1,2-dichloro-ethane;